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C1 APPENDIX C Dynamic Modulus Equipment Effects Data

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C2 Table C1. Dynamic modulus data for ITC equipment. Load Deformation Conf Dynamic Phase Standard Deformation Standard Deformation Phase Specimen Temp Freq Pressure Modulus Angle Error Drift Error Uniformity Uniformity C Hz KPa MPa % % % % 109 10 10 0 11006 15.6 3.5 134.5 6.7 24.0 0.2 109 10 1 0 7019 22.0 0.6 169.3 5.6 31.9 0.8 109 10 0.1 0 3874 28.3 0.3 203.4 4.6 33.8 1.4 114 10 10 0 11193 15.6 3.2 144.4 6.5 32.9 0.5 114 10 1 0 7106 22.3 0.5 193.4 5.8 36.6 0.3 114 10 0.1 0 3893 28.8 0.5 237.2 6.1 35.7 1.2 115 10 10 0 9636 15.3 4.0 127.5 6.3 12.2 0.5 115 10 1 0 6297 21.3 0.9 153.4 5.1 9.9 0.6 115 10 0.1 0 3555 27.3 0.7 174.2 5.6 16.1 1.0 118 10 10 0 11857 15.2 2.9 140.4 6.1 11.6 0.1 118 10 1 0 7602 21.4 0.5 187.6 5.3 10.5 0.1 118 10 0.1 0 4202 27.2 1.3 243.0 5.3 4.8 0.2 109 20 10 0 5959 25.4 5.5 357.4 22.0 36.4 0.0 109 20 1 0 3038 31.9 1.4 359.0 14.9 33.2 0.0 109 20 0.1 0 1376 34.3 1.4 262.5 5.9 22.4 0.3 114 20 10 0 6128 25.3 5.1 355.5 22.5 44.9 0.2 114 20 1 0 3152 31.8 1.3 333.2 15.2 47.1 2.0 114 20 0.1 0 1429 34.7 2.8 193.9 7.5 43.5 3.8 115 20 10 0 6202 25.9 5.4 384.4 20.5 15.9 0.5 115 20 1 0 2997 32.9 1.4 444.9 15.8 15.2 0.9 115 20 0.1 0 1312 36.4 4.0 359.4 8.4 15.0 1.8 118 20 10 0 6481 26.1 5.1 413.6 21.8 16.3 0.3 118 20 1 0 3233 33.2 1.4 477.8 16.2 22.5 0.1 118 20 0.1 0 1448 36.9 4.4 433.4 11.2 31.3 0.8 109 35 10 0 1864 34.6 7.4 268.4 11.5 15.7 0.6 109 35 1 0 782 32.3 2.5 114.6 5.7 8.3 1.0 109 35 0.1 0 383 25.0 5.5 55.0 7.3 1.1 1.3 109 35 0.01 0 255 17.2 3.2 31.3 6.2 10.1 1.6 114 35 10 0 2036 35.1 7.9 316.0 12.4 14.6 0.8 114 35 1 0 846 33.7 2.2 176.9 5.6 6.4 0.7 114 35 0.1 0 404 26.8 4.5 96.6 6.5 1.7 0.1 114 35 0.01 0 222 18.4 3.2 27.5 5.8 13.8 0.2 115 35 10 0 1902 35.3 8.8 350.2 12.4 0.5 1.2 115 35 1 0 802 34.1 2.5 242.9 6.4 4.1 2.0 115 35 0.1 0 399 27.1 5.0 197.2 6.2 10.2 2.0 115 35 0.01 0 262 18.2 3.2 83.5 6.2 30.4 0.1 118 35 10 0 2149 36.0 8.3 368.4 13.3 29.2 1.1 118 35 1 0 879 35.1 2.8 219.3 6.8 20.8 0.5 118 35 0.1 0 404 27.8 4.6 136.5 6.2 11.1 0.3 118 35 0.01 0 240 18.6 2.6 51.6 4.8 12.5 1.7 109 35 10 140 2535 29.7 7.7 180.6 9.9 43.7 1.4 109 35 1 140 1370 26.0 1.8 115.0 6.5 50.4 1.7

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C3 Table C1. (Continued). Load Deformation Conf Dynamic Phase Standard Deformation Standard Deformation Phase Specimen Temp Freq Pressure Modulus Angle Error Drift Error Uniformity Uniformity C Hz KPa MPa % % % % 109 35 0.1 140 923 20.1 4.4 103.8 7.4 52.5 2.0 109 35 0.01 140 733 14.1 1.2 79.8 6.9 54.6 1.9 114 35 10 140 2410 28.6 7.1 151.8 8.4 17.2 1.0 114 35 1 140 1342 24.7 1.7 100.5 5.2 8.1 1.6 114 35 0.1 140 918 18.8 2.8 87.0 4.6 0.5 1.0 114 35 0.01 140 742 13.1 1.5 70.3 5.4 2.4 0.1 115 35 10 140 2570 29.2 7.2 167.9 8.9 3.5 1.3 115 35 1 140 1403 25.0 1.7 100.9 5.3 5.3 1.7 115 35 0.1 140 953 19.4 1.7 87.3 5.0 13.1 0.9 115 35 0.01 140 762 13.2 8.1 67.7 10.0 17.8 0.7 118 35 10 140 2711 29.2 8.0 158.8 10.2 17.4 0.8 118 35 1 140 1468 25.2 2.1 91.4 6.6 10.5 1.0 118 35 0.1 140 988 19.1 5.0 80.7 8.2 5.1 0.3 118 35 0.01 140 798 12.8 15.6 60.1 17.9 1.8 0.2

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C4 Table C2. Dynamic modulus data for IPC equipment. Load Deformation Conf Dynamic Phase Standard Deformation Standard Deformation Phase Specimen Temp Freq Pressure Modulus Angle Error Drift Error Uniformity Uniformity C Hz kPa MPa % % % % 111 10 10 0 10268 16.1 3.4 -114.7 4.0 1.4 0.4 111 10 1 0 6527 21.9 2.8 -192.5 4.0 1.8 0.6 111 10 0.1 0 3611 28.1 1.6 -247.6 4.4 0.8 0.8 112 10 10 0 11044 15.6 3.2 -106.3 3.5 3.5 0.0 112 10 1 0 7107 20.8 8.6 -149.0 5.0 3.5 0.1 112 10 0.1 0 3955 26.5 1.6 -180.2 3.0 3.4 0.2 117 10 10 0 11486 15.9 3.7 -115.0 3.8 15.6 0.4 117 10 1 0 7307 21.7 2.6 -201.9 3.7 16.9 0.5 117 10 0.1 0 3992 28.4 1.7 -280.5 4.4 18.5 0.6 119 10 10 0 9949 16.3 4.0 -115.7 5.1 1.8 0.2 119 10 1 0 6237 22.1 2.8 -200.7 4.6 0.8 0.4 119 10 0.1 0 3380 28.6 1.7 -271.2 5.4 1.5 0.5 111 20 10 0 5299 26.0 2.8 -328.1 6.0 21.1 1.0 111 20 1 0 2594 32.9 1.5 -432.0 6.0 18.6 1.3 111 20 0.1 0 1113 36.5 1.3 -373.1 5.1 17.8 1.5 112 20 10 0 5938 23.9 4.1 -277.1 6.0 4.5 0.3 112 20 1 0 3092 30.4 1.5 -357.9 5.4 2.0 0.6 112 20 0.1 0 1360 34.6 1.2 -299.8 4.9 1.5 0.7 117 20 10 0 6171 25.0 4.7 -323.6 6.7 11.0 0.7 117 20 1 0 3127 32.1 1.4 -421.9 5.9 13.8 0.9 117 20 0.1 0 1335 36.0 1.3 -364.3 5.0 15.4 1.1 119 20 10 0 5485 25.0 3.2 -300.7 5.5 14.8 1.0 119 20 1 0 2767 31.8 1.5 -400.0 5.7 11.8 1.3 119 20 0.1 0 1180 35.8 1.3 -346.6 5.3 10.2 1.5 111 35 10 0 1952 34.9 5.4 -448.5 14.3 3.9 0.8 111 35 1 0 824 33.8 3.3 -156.0 5.1 4.2 1.5 111 35 0.1 0 313 30.0 3.6 -40.8 4.5 8.5 2.9 111 35 0.01 0 148 23.5 2.1 -4.6 6.8 19.0 4.7 112 35 10 0 2186 33.6 4.6 -369.2 11.7 8.4 1.0 112 35 1 0 942 32.5 3.0 -135.3 4.4 9.8 1.6 112 35 0.1 0 383 28.7 3.2 -35.1 5.7 12.3 2.3 112 35 0.01 0 191 22.2 1.8 14.4 6.8 19.3 3.7 117 35 10 0 2277 35.2 5.1 -506.4 14.7 5.1 0.4 117 35 1 0 963 34.3 2.9 -208.9 5.3 6.0 0.2 117 35 0.1 0 361 31.4 3.6 -73.3 4.9 6.3 0.8 117 35 0.01 0 168 24.2 1.9 -47.3 7.0 8.8 2.9 119 35 10 0 2059 35.0 4.9 -484.3 13.0 12.9 0.7 119 35 1 0 894 33.7 3.1 -211.1 5.4 12.1 1.0 119 35 0.1 0 372 29.5 3.2 -74.6 4.2 17.1 2.3 119 35 0.01 0 192 21.6 1.8 -35.8 6.5 28.7 6.4 111 35 10 140 2483 30.9 3.0 -345.2 8.3 13.8 1.1

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C5 Table C2. (Continued). Load Deformation Conf Dynamic Phase Standard Deformation Standard Deformation Phase Specimen Temp Freq Pressure Modulus Angle Error Drift Error Uniformity Uniformity C Hz kPa MPa % % % % 111 35 1 140 1336 27.1 2.5 -204.6 4.4 14.4 0.8 111 35 0.1 140 868 21.9 2.0 -199.1 5.7 13.9 0.9 111 35 0.01 140 698 16.0 0.9 -147.5 6.1 12.5 1.1 112 35 10 140 2268 31.6 5.2 -402.1 9.8 6.9 0.7 112 35 1 140 1233 28.2 2.5 -248.8 5.0 4.9 0.8 112 35 0.1 140 820 23.1 1.7 -181.6 5.1 4.0 0.9 112 35 0.01 140 685 16.8 0.8 -102.3 6.5 3.6 0.8 117 35 10 140 2438 30.9 3.3 -228.5 8.1 11.3 1.0 117 35 1 140 1275 25.8 2.1 -58.7 2.6 11.8 0.8 117 35 0.1 140 829 19.4 1.4 -30.4 2.9 11.5 0.7 117 35 0.01 140 679 13.8 0.8 -29.7 5.8 10.3 0.8 119 35 10 140 2271 30.4 2.8 -321.2 8.4 9.4 0.7 119 35 1 140 1245 26.2 2.0 -182.3 4.1 9.2 0.7 119 35 0.1 140 813 21.2 1.8 -140.0 4.7 9.4 0.6 119 35 0.01 140 664 15.6 0.8 -101.5 7.9 9.3 0.6

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C6 Table C3. Dynamic modulus data for MDTS equipment. Load Deformation Conf Dynamic Phase Standard Deformation Standard Deformation Phase Specimen Temp Freq Pressure Modulus Angle Error Drift Error Uniformity Uniformity C Hz kPa MPa % % % % 111 10 10 0 11336 16.8 0.4 51.2 2.3 18.8 0.9 111 10 1 0 7556 22.2 0.1 165.5 5.3 18.2 1.7 111 10 0.1 0 4178 26.8 0.0 221.3 5.4 9.7 4.5 113 10 10 0 13150 16.6 0.3 144.0 6.4 16.3 2.7 113 10 1 0 7841 24.7 0.2 186.6 4.2 0.4 1.9 113 10 0.1 0 3792 30.4 0.0 182.4 4.2 19.9 0.7 116 10 10 0 11961 16.6 0.5 115.6 2.8 21.6 4.4 116 10 1 0 7637 22.3 0.1 252.3 6.3 19.3 3.7 116 10 0.1 0 4242 27.4 0.0 257.4 7.2 16.6 4.3 120 10 10 0 11010 14.0 0.4 60.6 1.8 35.3 2.3 120 10 1 0 7610 22.4 0.1 156.2 3.7 28.6 0.3 120 10 0.1 0 3918 27.3 0.0 229.4 5.4 8.1 2.9 111 20 10 0 6359 21.2 0.7 129.3 4.1 22.7 0.7 111 20 1 0 3676 29.8 0.2 140.2 5.2 25.4 0.9 111 20 0.1 0 1694 32.8 0.1 87.6 4.6 24.5 1.3 113 20 10 0 6660 21.3 0.7 140.3 3.2 28.4 1.5 113 20 1 0 3002 30.4 0.3 221.4 6.2 5.6 0.6 113 20 0.1 0 1546 33.3 0.1 157.3 6.9 7.1 0.8 116 20 10 0 5818 18.3 0.7 85.7 2.5 32.8 4.7 116 20 1 0 3052 27.7 0.3 219.2 5.9 14.9 7.4 116 20 0.1 0 1417 32.1 0.1 136.0 6.1 6.8 4.7 120 20 10 0 5235 17.5 0.7 122.4 2.4 19.0 2.1 120 20 1 0 3307 27.6 0.3 174.3 3.6 15.9 0.0 120 20 0.1 0 1713 30.6 0.1 166.9 4.9 18.7 0.8 111 35 10 0 2138 32.2 1.3 157.3 2.7 2.3 6.5 111 35 1 0 850 32.0 0.7 76.7 4.9 2.9 8.4 111 35 0.1 0 399 27.5 0.3 50.4 6.1 24.0 1.2 111 35 0.01 0 234 22.1 0.3 100.5 10.3 46.6 5.2 113 35 10 0 2165 35.0 1.3 236.7 6.5 7.7 7.3 113 35 1 0 821 36.7 0.7 62.0 5.5 7.5 3.8 113 35 0.1 0 404 32.0 0.3 33.6 6.2 18.8 6.8 113 35 0.01 0 262 25.2 0.3 49.5 12.8 33.2 11.0 116 35 10 0 2033 32.9 1.4 324.1 11.3 4.0 6.5 116 35 1 0 890 32.1 1.0 80.5 6.1 2.6 0.9 116 35 0.1 0 392 27.3 0.3 59.7 6.3 6.0 3.5 116 35 0.01 0 236 21.1 0.3 80.2 11.3 16.0 7.5 120 35 10 0 1788 34.4 1.8 347.9 9.8 14.1 0.9 120 35 1 0 755 34.4 0.8 288.7 10.3 13.7 1.7 120 35 0.1 0 312 32.0 0.3 268.5 8.1 0.1 3.5 120 35 0.01 0 127 32.3 0.5 152.5 10.8 29.1 3.0 111 35 10 140 2240 30.4 1.0 137.7 3.3 4.8 1.2

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C7 Table C3. (Continued). Load Deformation Conf Dynamic Phase Standard Deformation Standard Deformation Phase Specimen Temp Freq Pressure Modulus Angle Error Drift Error Uniformity Uniformity C Hz kPa MPa % % % % 111 35 1 140 1123 26.8 0.3 10.8 2.6 12.4 0.7 111 35 0.1 140 714 19.8 0.1 13.2 2.9 13.7 0.5 111 35 0.01 140 555 13.8 0.1 24.2 3.8 12.2 0.3 113 35 10 140 2390 29.3 0.9 179.9 3.7 17.2 1.0 113 35 1 140 1196 26.1 0.4 131.0 3.0 22.3 2.1 113 35 0.1 140 780 19.4 0.1 98.2 3.5 23.5 2.4 113 35 0.01 140 680 15.2 0.6 106.0 15.1 41.1 4.4 116 35 10 140 2149 31.2 1.1 237.4 3.6 17.1 1.2 116 35 1 140 991 28.0 0.5 45.4 2.7 17.1 2.0 116 35 0.1 140 597 22.8 0.1 18.9 4.0 11.1 1.8 116 35 0.01 140 493 17.5 0.1 46.5 4.8 2.8 1.4 120 35 10 140 2190 31.7 1.3 203.3 4.2 4.1 2.4 120 35 1 140 1153 27.4 0.4 76.3 2.5 9.7 2.1 120 35 0.1 140 765 20.7 0.1 71.0 3.0 11.2 1.7 120 35 0.01 140 672 19.2 0.4 90.6 41.8 80.0 3.6