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NCHRP Report 696: Performance of Corrugated Pipe Manufactured with Recycled Polyethylene Content (2011)
National Cooperative Highway Research Program (NCHRP)

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Thomas, Richard W, Cuttino, David, Transportation Research Board. "Specifications." NCHRP Report 696: Performance of Corrugated Pipe Manufactured with Recycled Polyethylene Content. Washington, DC: The National Academies Press, 2011.

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Page
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Page
14
Front Matter (R1-R11)
Summary (1-2)
Chapter 1 - Introduction (3-3)
Short-Term Properties (4-4)
Service Lifetime of PE (5-7)
The SIM for Predicting Creep and Creep Rupture (Stage I) Properties (8-11)
The FL-DOT Junction Test (12-12)
The Long-Term Oxidation (Stage III) Resistance (13-13)
Specifications (14-14)
Post-Industrial Recycled Polyethylene (15-15)
Post-Consumer Recycled High-Density Polyethylene (16-16)
PCR Mixed-Color Resin (17-17)
The Effects of Contamination (18-18)
The Effects of Melt Filtration (19-20)
The Effect of Silicone Rubber (21-23)
Phase 2 - Recycled-Resin Blends (24-25)
Blends Made with Mixed-Color PCR (26-27)
Blends Made with Natural PCR (28-29)
Blends Made with PIR-HD (30-31)
Index Test Results (32-33)
Stress-Crack Test Results (34-36)
Long-Term Tensile Strength by SIM (37-39)
Long-Term Creep Strain and Modulus by SIM (40-40)
Long-Term Stress-Crack Resistance (41-41)
Combined SIM (Stage I) and BFF (Stage II) Service-Lifetime Estimates (42-44)
The BFF Test for QC (45-45)
Designing Pipe with Recycled Content (46-46)
Proposed Draft Specifications (47-48)
Phase 2 - Recycled PE Blends (49-49)
Phase 3 - Pipe Made from Recycled-Resin Blends (50-53)
References (54-54)
Appendix A - Procedures and Test Methods (55-55)
A.2.4 Percentage Black/Color + Ash (ASTM D4218) (56-56)
A.2.6 Percentage Polypropylene (TRI Method) (57-58)
A.2.8 Flexural Modulus (ASTM D790) (59-59)
A.3.2 BAM Stress-Crack Test (TRI Method) (60-61)
A.3.3 BFF Test (TRI Method) (62-62)
A.3.4 Junction Test (FDOT FM 5-572) (63-63)
A.4.1 Stepped Isothermal Method (SIM) For Long-Term Creep Modulus and Strain (ASTM D6992) (64-64)
A.4.3 BFF Test for Long-Term Stress Crack Resistance (TRI Method) (65-68)
Appendix D - Pipe Containing Recycled HDPE (69-69)
Appendix E - Proposed Draft Standard Specification for PCR MCR High-Density PE Bottles for Use in AASHTO-Approved Corrugated Drainage Pipe (70-76)
Appendix F - Proposed Draft Standard for Recycled Content Containing HDPE Resin Formulations for Corrugated Pipe Made to AASHTO Standard M252-Recycled (77-84)
Appendix G - Proposed Draft Standard Specification for Recycled Content Containing HDPE Resin Formulations for Corrugated Pipe Made to AASHTO Standard M294-Recycled (85-93)
Appendix H - Proposed Draft Standard Specification for Corrugated Polyethylene Drainage Pipe Containing Recycled Polyethylene, 75- to 250-mm Diameter (94-108)
Appendix I - Proposed Draft Standard Specification for Corrugated Polyethylene Drainage Pipe Containing Recycled Polyethylene, 300- to 1,500-mm Diameter (109-129)
Abbreviations used without definitions in TRB publications (130-130)

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14 1,000 ppm Irgaphos 168, the OIT value will be around 70 min- blends and only buy high quality reprocessed recycled material utes and the pipe will be well stabilized. from the recycled suppliers. Because of this complicated way in which recycled resin may make its way into AASHTO approved pipe, there could be up to five different specifications. Specifications First, one may need a specification for post-consumer recy- Ensuring consistent properties for blends containing recycled cled, mixed-color reprocessed (PCR-MCR) HDPE in pellet resins will be challenging. There are a number of different form. This will be used by compounders and corrugators to kinds of companies that will be involved once AASHTO allows ensure that they are receiving a consistent stream of material recycled use. from which to make recycled blends. Its focus will be mostly At the beginning of the process are the recycled-resin on how well the material is melt filtered and how much suppliers. These companies specialize in locating, cleaning, polypropylene is present, among other things. These are reprocessing, and selling recycled materials. Some are small believed to be important properties for good recycled material. family-owned businesses that simply grind and clean recycled Then there may be two specifications for fully formulated materials while others are fairly sophisticated with auto- recycled content­containing blends. One will be for use in pipe mated cleaning and optical color sorting. And there are many for AASHTO M252 and drainage applications and the other in-between. Some will be happy just selling reprocessed re- for M294 applications. Apparently, these two applications are cycled HDPE and others will want to prepare and sell fully different enough that a different quality and type of resin is formulated blends directly to the corrugated pipe manufac- used for each one. These are necessary for the corrugators to turer. Next will be the compounders. This group may include know what is being purchased to be converted to pipe. the recycled-resin supplier, but other companies with estab- Finally, there will also be two specifications--M252-Recycled lished sources of sub-prime virgin resins will use their blending and M294-Recycled--for pipe made from recycled content­ and formulating technology to make fully formulated recycled containing resins. These specifications will include both resin blends for direct sales to the corrugators. And, finally, some properties and the properties of the final pipe; all testing will pipe manufacturers themselves may want to prepare their own be conducted on the pipe or on samples taken from the pipe.