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NCHRP Report 696: Performance of Corrugated Pipe Manufactured with Recycled Polyethylene Content (2011)
National Cooperative Highway Research Program (NCHRP)

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Thomas, Richard W, Cuttino, David, Transportation Research Board. "Long-Term Stress-Crack Resistance." NCHRP Report 696: Performance of Corrugated Pipe Manufactured with Recycled Polyethylene Content. Washington, DC: The National Academies Press, 2011.

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Page
41
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41
Front Matter (R1-R11)
Summary (1-2)
Chapter 1 - Introduction (3-3)
Short-Term Properties (4-4)
Service Lifetime of PE (5-7)
The SIM for Predicting Creep and Creep Rupture (Stage I) Properties (8-11)
The FL-DOT Junction Test (12-12)
The Long-Term Oxidation (Stage III) Resistance (13-13)
Specifications (14-14)
Post-Industrial Recycled Polyethylene (15-15)
Post-Consumer Recycled High-Density Polyethylene (16-16)
PCR Mixed-Color Resin (17-17)
The Effects of Contamination (18-18)
The Effects of Melt Filtration (19-20)
The Effect of Silicone Rubber (21-23)
Phase 2 - Recycled-Resin Blends (24-25)
Blends Made with Mixed-Color PCR (26-27)
Blends Made with Natural PCR (28-29)
Blends Made with PIR-HD (30-31)
Index Test Results (32-33)
Stress-Crack Test Results (34-36)
Long-Term Tensile Strength by SIM (37-39)
Long-Term Creep Strain and Modulus by SIM (40-40)
Long-Term Stress-Crack Resistance (41-41)
Combined SIM (Stage I) and BFF (Stage II) Service-Lifetime Estimates (42-44)
The BFF Test for QC (45-45)
Designing Pipe with Recycled Content (46-46)
Proposed Draft Specifications (47-48)
Phase 2 - Recycled PE Blends (49-49)
Phase 3 - Pipe Made from Recycled-Resin Blends (50-53)
References (54-54)
Appendix A - Procedures and Test Methods (55-55)
A.2.4 Percentage Black/Color + Ash (ASTM D4218) (56-56)
A.2.6 Percentage Polypropylene (TRI Method) (57-58)
A.2.8 Flexural Modulus (ASTM D790) (59-59)
A.3.2 BAM Stress-Crack Test (TRI Method) (60-61)
A.3.3 BFF Test (TRI Method) (62-62)
A.3.4 Junction Test (FDOT FM 5-572) (63-63)
A.4.1 Stepped Isothermal Method (SIM) For Long-Term Creep Modulus and Strain (ASTM D6992) (64-64)
A.4.3 BFF Test for Long-Term Stress Crack Resistance (TRI Method) (65-68)
Appendix D - Pipe Containing Recycled HDPE (69-69)
Appendix E - Proposed Draft Standard Specification for PCR MCR High-Density PE Bottles for Use in AASHTO-Approved Corrugated Drainage Pipe (70-76)
Appendix F - Proposed Draft Standard for Recycled Content Containing HDPE Resin Formulations for Corrugated Pipe Made to AASHTO Standard M252-Recycled (77-84)
Appendix G - Proposed Draft Standard Specification for Recycled Content Containing HDPE Resin Formulations for Corrugated Pipe Made to AASHTO Standard M294-Recycled (85-93)
Appendix H - Proposed Draft Standard Specification for Corrugated Polyethylene Drainage Pipe Containing Recycled Polyethylene, 75- to 250-mm Diameter (94-108)
Appendix I - Proposed Draft Standard Specification for Corrugated Polyethylene Drainage Pipe Containing Recycled Polyethylene, 300- to 1,500-mm Diameter (109-129)
Abbreviations used without definitions in TRB publications (130-130)

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41 3 Sample B1 2.22 % 2.5 2.15 % 2 STRAIN (%) REFERENCE TEMPERATURE - 23C 1.5 100 Yrs 500 psi Stress 1 50 Yrs 0.5 0 -4 -3 -2 -1 0 1 2 3 4 5 6 7 LOG TIME (hr) Figure 40. Creep strain master curve for Sample B1. 200000 180000 Sample B1 160000 50 Yrs 100 Yrs CREEP MODULUS (psi) 140000 120000 100000 80000 60000 23,250 psi 40000 22,531 psi REFERENCE TEMPERATURE - 23C 20000 500 psi Stress 0 -3 -2 -1 0 1 2 3 4 5 6 7 8 LOG TIME (hr) Figure 41. Creep modulus master curve for Sample B1. Next, the SIM was used to determine the creep properties The raw data and the master creep curves for these samples of the samples when placed under an applied stress of 500 psi. are found in Appendix D, Section D.12. These results will be This involves a series of 10,000 second (166 min) creep tests, used to evaluate how one would design with recycled formu- each done on the same test specimen and separated by 7°C lations in the context of Section 12 of the AASHTO LRFD in temperature. In this case, creep curves were generated Bridge Design Specifications (15). from 20°C to 83°C. The raw data are then shifted through TTS to generate a master creep curve at a reference tempera- Long-Term Stress-Crack Resistance ture (23°C). Creep strain and creep modulus master curves for sample B1 (100% VR1) are shown in Figures 40 and 41, The six final candidate formulations and the PCR MCR resin and all of the results are shown in Table 17. were evaluated by the BFF test under the three sets of conditions Table 17. Long-term creep strain and creep modulus under 500 psi of stress. Creep Strain Creep Modulus Sample 50 year 100 year 50 year 100 year B1 2.15 2.22 23,250 22,531 A2 2.07 2.14 24,160 23,358 L5 2.22 2.30 22,549 21,719 A5 2.19 2.26 22,821 22,091 B3 2.24 2.32 22,300 21,532 B5 2.64 2.72 18,965 18,406