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OCR for page 124
Appendix C
Choice of Chemical Constituents
124
OCR for page 125
Appendix C
125
TABLE 3.2 -- Major metals and trace elements targeted for analysis in
tissues collected in the National Water--Quality Assessment Program and
currently analyzed in existing tissue analysis programs of national scope
Program
Name of
metal or
element
National
Water-
Quality
Assessment
Program
National
Status and National
Trends Bioaccumula-
Program tion Study
(NOAA)2
(EPA)3
National
Contami-
tant
Biomoni-
toring
Program
(FWS)4
-
.
Aluminum
Antimony
Arsenic
Barium
Beryllium +
Cadmium
+
Chromium +
Copper +
Iron
Lead
Manganese
Mercury
Molybdenum +
Nickel
Selenium
Silicon
Silver
Thallium
Tin
Vanadium
Zinc
+
+
+
+
+
+
+
+
+
+
+
+
+
+
1U.S. Geological Survey
2National Oceanic and Atmospheric Administration
3U.S. Environmental Protection Agency
4U.S. Fish and Wildlife Service
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126
NAWQA Pilot Program
TABLE 3.3 -- Synthetic organic compounds targeted for analysis in tissues
collected in the National Water-Quality-Assessment Program and currently
analyzed in existing tissue analysis programs of national scope
Pro~ram
-
National
National Contami-
Water- National tent
Name of Quality Status and National Biomoni-
metal or Assessment Trends Bioaccumula- toring
element Program Program tion Study Program
(USGS)1 (NOAA)2 (EPA)3 (FWS)4
Polynuclear aromatic
hYdrocarbons
Acenaphthene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene +
Benzo(e)pyrene
Biphenyl
Chrysene
Dibenz(a,h)anthra-
+
+
. +
cene
2,6-Dimethylnaph
thalene
Fluoranthene +
Fluorene +
1-Methyluaphthalene
2-Methylnaphthalene
1-Methylphenan-
threne
Naphthalene
Perylene
Phenanthrene
Pyrene
Organochlorine
insecticides
Aldrin
Butachlor
Chlorbenzilate
Chlordane, cis
Chlordane, bans
+
t
+
+
t
+
+
+
+
+
+
+
+
+
+
+
OCR for page 127
Appendix C
TABLE 3.3 -- continued
127
National
National Contami-
Water- National tent
Name of Quality Status and National Biomoni-
metal or Assessment Trends Bioaccumula- toring
element Program Program tion Study Program
(USGS)1 (NOM )2 (EPA)3 (FWS)4
Organochlorine
insecticides
- continued
Chlorpyrifos + + +
o,p'-DDD + + +
p,p'-DDD + + +
c,p'-DDE + +
p,p'-DDE + + + +
o,p'-DDT + +
o,p'-DDT + +
Dicofol (Kelthane) + + +
Dieldrin + + + +
Diethylhexylphtha-
late (DEHP) + + +
Diphenyldisulfide + + +
Endrin + + +
Heptachlor + + + +
Heptachlor epoxide + + + +
Hexachlorobenzene
(HCB) + + + +
Hexachlorocyclo-
hexanes (BHC) +
including Lindane
+
+
+
Isopropalin + + +
Kepone + + +
Mercury, organic + + +
Methoxychlor + + +
Mirex + + + +
n-aLkanes + + +
Nitrofen + + +
Nonachlor, cis + + +
Nonachlor, bans + + + +
Octachlorostyrene + + +
Oxychlordane + + +
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128
TABLE 3.3 -- continued
NA WQA Pilot Program
Program
National
National Contami-
Water- National tent
Name of Quality Status and National Biomoni-
metal or Assessment Trends Bioaccumula- toring
element Program Program tion Study Program
(USGS)1 (NOAA)2 (EPA)3 (FWS)4
.
Organochlorine insecticides - continued
Pentachloroani-
sole
Pent a chloro -
benzene
Pentachloro-
+
+
nitrobenzene
(PCNB)
Pent achloro -
phenol (PCP)
Perthane
1,2,4,5-Tetra-
chlorobenzene +
1,2,3,4-Tetrachloro-
benzene
1,2,3,5-Tetrachloro-
+
+
+
+
+
+
+
+
+
benzene + + +
Toxaphene +
1,2,3-Trichloro-
benzene + + +
1,2,4-Trichloro-
benzene + + +
1,3,5-Trichloro-
benzene + + +
Trichloronate
Trifluralin
Triphenyl phosphate +
PolYchlorinated biphenyl
s
+
Monochlorobiphenyls +
Dichlorobiphenyls + + +
Trichlorobiphenyls + + +
Tetrachlorobiphenyls + + +
+
+
+
+
+
+
+
OCR for page 129
Appendix C
TABLE 3.3 -- continued
129
Pro~ram
National
National Contami-
Water- National tent
Name of Quality Status and National Biomoni-
metal or Assessment Trends Bioaccumula- toring
element Program Program tion Study Program
(USGS)1 (NO M )2 (EPA)3 (FWS)4
PolYchlorinated biphenyls - continued
Pentachlorobiphenyls + + +
Hexachlorobiphenyls + + +
Hepatachloro-
biphenyls + + +
Octachlorobiphenyls + + +
Nonachlorobiphenyls + + +
Decachlorobiphenlys +
3,4,3',4'-Tetra-
chlorobiphenyl +
3,4,5,3',4'-Penta-
chlorobiphenyl +
3,4,5,3',4',5'-Hexa-
chlorobiphenyl +
Total PCBs + +
Aroclor 1242 +
Aroclor 1248 +
Aroclor 1254 +
Aroclor 1260 +
Chlorinated Dioxins and
Furans
2,3,7,8-TCDD +
1,2,3,7,8-PeDD +
1,2,3,6,7,8-HxDD +
1,2,3,7,8,9-HxDD +
1,2,3,7,8-HxDD +
1,2,3,4,6,7,8-HpDD +
2,3,7,8-TCDF +
1,2,3,7,8-PeDF +
2,3,4,7,8-PeDF +
1,2,3,6,7,8-HxDF +
1,2,3,7,8,9-HxDF +
1,2,3,4,7,8-HxDF +
2,3,4,6,7,8-HxDF +
1,2,3,4,6,7,8-HxDF +
1,2,3,4,7,8,9-HxDF +
1U.S. Geological Survey
2National Oceanic and Atmospheric Administration
3U.S. Environmental Protection Agency
4U.S. Fish and Wildlife Service
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130
NAWQA Pilot Program
TABLE 3.4 -- Semi-volatile, methylene-chloride extractable target compounds
to be determined in the <2 millimeter fraction of selected bed-material
samples from the surface-water part of the National Water-Quality
Assessment Program. (U.S. Geological Survey National Water Quality
Laboratory Schedule 1386 for total recoverable compounds) [Reporting level
is in micrograms per liter]
Compound
CAS No.
WATSTORE
Code
Reporting
Level
4-Chloro-3-methylphenol
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4 Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2, 4,6-Trichlorophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo (a) anthracene
Benzo (b) flouranthene
Benzo (k) flouranthene
Benzo (g,h,i) perylene
Benzo (a) pyrene
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
his (2-Chloroethoxy) methane
bis (2-Chloroethyl) ether
bis (2-Chloroisopropyl) ether
59-50-7
95-57-8
120-83-2
105-67-9
534-52-1
51-28-5
88-75-5
100-02-7
87-86-5
08-95-2
88-06-2
83-32-9
208-96-8
120-12-7
56-55-3
205-99-2
207-08-9
191-24-2
50-32-8
101-55-3
85-68-7
111-91-1
111-44-4
180-60-1
34455
34589
34604
34609
34660
34619
34594
34649
39061
34695
34624
34208
34203
34223
34529
34233
34245
34524
34250
34639
34295
34281
34276
34286
600
200
200
200
600
600
200
600
600
200
600
200
200
200
200
400
400
400
400
200
200
200
200
200
OCR for page 131
Appendix C
TABLE 3.5 -- Target organochlorine compounds to be determined in the <2
millimeter fraction of selected bed-material samples from the surface-
water part of the National Water-Quality Assessment Program. (U. S.
Geological Survey National Water-Quality Laboratory Schedule 1325 for
total-recoverable compounds) "Reporting, level is in micrograms per liter]
WATSTORE Reporting
Compound CAS No. Code Level
Aldrin 309-00-2 39333 0 ~ 01
5103-74-2
Chlordane 5103-71-9 39351 1.00
ODD 72-54-8 39363 0.10
ODE 72-55-9 39368 0.10
DOT 50-29-3 39373 0.10
Dieldrin 60-57-1 39383 0.10
Endosulfan 115-29-7 39389 0.10
Endrin 72-20-8 39393 1.00
Gross PCBs 39519 1.00
Gross PCNs 39251 1.00
Heptachlor 76-44-8 39413 0.10
Heptachlor epoxide 1024-57-3 39423 0.10
Lindane 58-89-9 39343 0.10
Methoxychlor 72-43-5 39481 0.10
Mirex 2385-85-5 39758 0.10
Perthane 72-56-0 81886 1.00
Toxaphene 8001-35-2 39403 10.00
131
OCR for page 132
132
NAWQA Pilot Program
TABLE 3.6 -- Target acid-extractable organic compounds to be determined in
selected surface-water samples of the National Water-Quality Assessment
Program. (U.S. Geological Survey National Water-Quality Laboratory
Schedule 1393 for total-recoverable compounds) [Reporting level is in
micrograms per liter]
WATSTORE Reporting
Compound CAS No. Code Level
4-Chloro-3-methylphenol 59-50-7 34452 30.0
2-Chlorophenol 95-57-8 34586 5.0
2,4-Dichlorophenol 120-83-2 34601 5.0
2,4-Dimethylphenol 105-67-9 34606 5.0
2,4-Dinitrophenol 51-28-5 34616 20.0
4,6-Dinitro-2-methylphenol 534-52-1 34657 30.0
2-Nitrophenol 88-75-5 34591 5.0
4-Nitrophenol 100-02-7 34646 30.0
Pentachlorophenol 87-86-5 39032 30.0
Phenol 108-95-2 34694 5.0
2, 4,6-Trichlorophenol 88-06-2 34621 20.0
l
OCR for page 133
Appendix C
TABLE 3.7 -- Target organophosphorus insecticides to be determined in
selected surface-water samples of the National Water-Quality Assessment
Program. (U.S. Geological Survey National Water-Quality Laboratory
Schedule 1319 for total-recoverable compounds) [Reporting level is in
micrograms per liter]
133
WATSTORE Reporting
Compound CAS No. Code Level
Chlorpyrifos 38932 0.01
Diazinon 333-41-5 39570 0.01
Ethion 563-12-2 39398 0.01
Malathion 121-75-5 39530 0.01
Methyl parathion 298-00-0 39600 0.01
Methyl trithion 953-17-3 39790 0.01
Parathion 56-38-2 39540 0.01
Trithion 786-19-6 39786 0.01
1
OCR for page 134
134
NAWQA Pilot Program
TABLE 3.8 -- Target carbamate pesticides to be determined in selected
ground-water samples of the National Water Quality Assessment Program.
(U.S. Geological Survey National Water-Quality Laboratory Schedule SH13 for
total recoverable compounds ) [Reporting level is in micrograms per liter]
Compound
WATSTORE Reporting
CAS No. Code Level
Aldi c arb
Aldicarb sulfane
Aldicarb sulfoxide
Carbaryl
Carbofuran
3 -Hydroxyc arbofuran
Methiocarb
Methomyl
1-Napthol
Oxanyl
Propham
Propoxur (Baygon )
116-06-3 0.5
1646-88-4 0.5
1648-87-3 0.5
63-25-2 39750 0.5
1563-66-2 0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
2032-65-7
16752-77-5 39051
23135-22-0
122-42-9 39052
114-26- 1
OCR for page 135
Appendix C
135
TABLE 3.9 -- Target triazine and other nitro';en-containing herbicides to be
determined in selected surface- and ~,round-water samples from the National
Water-Quality Assessment Program. (U.S. Geological Survey National Water-
Quality Laboratory Schedule 1389 for total recoverable compounds)
[Reporting level is in micrograms per liter]
WATSTORE Reporting
Compound CAS No. Code Level
Alachlor 15972-60-8 77825 0.1
Ametryn 834-12-8 82184 0.1
Atrazine 1912-24-9 39630 0.1
Bromacil* 314-40-9
Butylate* 2008-41-5
Carboxin* 5234-68-4
Cyanazine 21725-46-2 81757 0.1
Cycloate* 1134-23-2
Diphenamid* 957-51-7
Hexazinone* 51235-04-2
Metolachlor 51218-45-2 39356 0.1
Metribuxin 21087-64-9 81408 0.1
Prometon 1610-18-0 39056 0.1
Prometryn 7287-19-6 39057 0.1
Propezine 139-40-2 39024 0.1
Simazine 122-34-9 39055 0.1
Simetryn 1014-70-6 39054 0.1
Terbacil* 5902-51-2
Trifluralin 1582-09-8
*Under development
OCR for page 136
136
NAUSEA Pilot Program
TABLE 3.10 -- Target chlorophenoxy acid herbicides to be determined in
selected surface- and ~,round-water samples of the National Water-Quality
Assessment Program. (U.S. Geological Survey National Water-Quality
Laboratory Schedule 0079 for total recoverable compounds ) "Reporting level
is in micrograms per liter]
WATSTORE Reporting
Compound CAS No. Code Level
2,4-D 94-75-7 39730 0.01
Dicamba 1918-00-9 82052 0.01
2, 4-DP 120-36-5 82183 0. 01
Picloram 1918-02-1 39720 0.01
Silvex 93-72-1 39760 0. 01
2, 4, 5-T 93-76-5 39740 0.01
OCR for page 137
Appendix C
TABLE 3.11 -- Target volatile organic compounds to be determined in
selected surface- and ground-water samples of the pilot National Water-
Quality Assessment Program. (U.S. Geological Survey National Water-
Quality Laboratory Schedule 1390 for total recoverable compounds)
[Reporting level is in micrograms per liter]
137
Compound
WATSTORE
Code
Reporting
Level
Bromodichloromethane 32101 0.2
Carbon tetrachloride 32102 0.2
1,2-Dichloroethane 32103 0.2
Bromoform 32104 0.2
Dibromochloromethane 32105 0.2
Chloroform 32106 0.2
Toluene 34010 0.2
Benzene 34030 0.2
Chlorobenzene 34301 0.2
Chloroethane 34311 0.2
Ethylbenzene 34371 0.2
Bromomethane 34413 0.2
Chloromethane 34418 0.2
Methylene chloride 34423 0.2
Tetrachloroethene 34475 0.2
Trichlorofluoromethane 34488 0.2
1,1-Dichloroethane 34496 0.2
1,1-Dichloroethene 34501 0.2
1, 1,1-Trichloroethane 34506 0.2
1, 1,1-Trichloroethene 34511 0.2
1, 1, 2,2-Tetrachloroethane 34516 0.2
1,2-Dichlorobenzene 34536 0.2
1,2-Dichloropropane 34541 0.2
1,2-Trans-dichloroethene 34546 0.2
1,2, 4-Trichlorobenzene 34551 0.2
1,3-Dichlorobenzene 34566 0.2
1,4-dichlorobenzene 34571 0.2
2-Chloroethylvinyl ether 34576 0.2
Dichlorodifluoromethane 34668 0.2
1,3-Trans-dichloropropene 34699 0.2
1,3-Cis-dichloropropene 34704 0.2
1,2-Dibromoethane 39082 0.2
Vinyl chloride 39175 0.2
Trichlorethene 39180 0.2
Hexachlorobutadiene 39702 0.2
1,2-Cis-dichloroethene 77093 0.2
Styrene 77128 0.2
OCR for page 138
138
TABLE 3.11 -- continued-
NAWQA Pilot Program
Compound
WATSTORE
Code
Reporting
Level
P-xylene 77133 0.2
M-xylene 77134 0 . 2
O-xylene 77135 0. 2
1,1-Dichloropropene 77168 0.2
1, 3-Dichloropropane 77173 0.2
1, 2, 4-Trimethylbenzene ~ 77222 0 .2
Isopropyl benzene 77223 0.2
N-propylbenzene 77224 0.2
1, 3, 5-Trimethylbenzene 77226 0 .2
O-chlorotoluene 77275 0. 2
P-chlorotoluene 77277 0. 2
Bromochloromethane 77297 0.2
N-butylbenzene 77342 0 .2
Sec-butylbenzene 77350 0.2
Tert-butylbenzene 77353 0 . 2
1, 2, 3-Trichloropropane 77443 0 .2
1, 1, 1, 2-tetrachloroethane 77562 0 .2
1, 2, 3-Trichlorobenzene 77613 0 .2
Bromobenzene 81555 0.2
1, 2-Dibromo-3-chloropropane 82625 0 .2
Napthalene 91203 0.2
P-isopropyl toluene --- 0.2
2, 2-Dichloropropene --- 0. 2
Representative terms from entire chapter:
geological survey
