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L-1 APPENDIX L Source of Data: AASHTO Materials Reference Laboratory Proficiency Sample Program Final Report Issued January 2001 Participation: 39 Total Laboratories 1 Laboratories Determined to be Invalid 4 Laboratories Determined to be Outliers 34 Total Laboratories Included in Analysis Sample 181 Sample 182 CV% CV% Average Average (181) (182) 0.703 26.390.263 0.743 28.93 0.249 10.85 10.46 1s d2s 0.908 0.942 0.099 0.279 CV% 1s Reproducibility (Sample 182)Reproducibility (Sample 181) d2s CV% 1s d2s Sa m pl e 18 2 Average Results Graph and Analysis Results for AASHTO T314 / D6723 (Strain) AMRL Performance Graded Binder Samples 181 and 182 AMRL Performance Graded Binder Samples 181 and 182 Determining the Fracture Properties of Asphalt Binder in Direct Tension Sample 181 Asphalt Grade: PG 64-16 / AC 10 Repeatability Lines With Small Dash Marks - Sample Outlier Boundaries Lines With Alternating Dash Marks - Sample Medians Line With Large Dash Marks - Center Diagonal Black Hexagon - Data Within is Used for Analysis Graph Legend -0.556 0.054 0.664 1.274 1.884 -0.939 -0.189 0.561 1.311 2.061 2.811
L-2 Source of Data: AASHTO Materials Reference Laboratory Proficiency Sample Program Final Report Issued June 2001 Participation: 47 Total Laboratories 0 Laboratories Determined to be Invalid 3 Laboratories Determined to be Outliers 44 Total Laboratories Included in Analysis Sample 183 Sample 184 CV% CV% Average Average (183) (184) 2.025 38.710.651 1.841 35.53 0.716 13.35 13.22 1s d2s 1.832 1.849 0.245 0.692 CV% 1s Reproducibility (Sample 184)Reproducibility (Sample 183) d2s CV% 1s d2s Sa m pl e 18 4 Average Results Graph and Analysis Results for AASHTO T314 / D6723 (Strain) AMRL Performance Graded Binder Samples 183 and 184 AMRL Performance Graded Binder Samples 183 and 184 Determining the Fracture Properties of Asphalt Binder in Direct Tension Sample 183 Asphalt Grade: PG 70-22 / -- Repeatability Lines With Small Dash Marks - Sample Outlier Boundaries Lines With Alternating Dash Marks - Sample Medians Line With Large Dash Marks - Center Diagonal Black Hexagon - Data Within is Used for Analysis Graph Legend -3.45 -1.302 0.846 2.994 5.142 7.29 -3.23 -1.169 0.892 2.953 5.014 7.075
L-3 Source of Data: AASHTO Materials Reference Laboratory Proficiency Sample Program Final Report Issued February 2002 Participation: 53 Total Laboratories 0 Laboratories Determined to be Invalid 0 Laboratories Determined to be Outliers 53 Total Laboratories Included in Analysis Sample 185 Sample 186 CV% CV% Average Average (185) (186) 1.034 25.160.344 0.974 24.99 0.366 12.24 11.61 1s d2s 1.378 1.453 0.169 0.477 CV% 1s Reproducibility (Sample 186)Reproducibility (Sample 185) d2s CV% 1s d2s Sa m pl e 18 6 Average Results Graph and Analysis Results for AASHTO T314 / D6723 (Strain) AMRL Performance Graded Binder Samples 185 and 186 AMRL Performance Graded Binder Samples 185 and 186 Determining the Fracture Properties of Asphalt Binder in Direct Tension Sample 185 Asphalt Grade: PG 64-22 / AC 20 Repeatability Lines With Small Dash Marks - Sample Outlier Boundaries Lines With Alternating Dash Marks - Sample Medians Line With Large Dash Marks - Center Diagonal Black Hexagon - Data Within is Used for Analysis Graph Legend -1.296 -0.206 0.884 1.974 3.064 4.154 -1.123 -0.133 0.857 1.847 2.837 3.827
L-4 Source of Data: AASHTO Materials Reference Laboratory Proficiency Sample Program Final Report Issued May 2002 Participation: 58 Total Laboratories 1 Laboratories Determined to be Invalid 3 Laboratories Determined to be Outliers 54 Total Laboratories Included in Analysis Sample 187 Sample 188 CV% CV% Average Average (187) (188) 3.474 40.931.292 3.655 43.59 1.228 9.67 9.55 1s d2s 2.965 3.001 0.287 0.811 CV% 1s Reproducibility (Sample 188)Reproducibility (Sample 187) d2s CV% 1s d2s Sa m pl e 18 8 Average Results Graph and Analysis Results for AASHTO T314 / D6723 (Strain) AMRL Performance Graded Binder Samples 187 and 188 AMRL Performance Graded Binder Samples 187 and 188 Determining the Fracture Properties of Asphalt Binder in Direct Tension Sample 187 Asphalt Grade: PG 76-22 / -- Repeatability Lines With Small Dash Marks - Sample Outlier Boundaries Lines With Alternating Dash Marks - Sample Medians Line With Large Dash Marks - Center Diagonal Black Hexagon - Data Within is Used for Analysis Graph Legend -5.19 -1.926 1.338 4.602 7.866 11.13 -6.52 -2.704 1.112 4.928 8.744
L-5 Source of Data: AASHTO Materials Reference Laboratory Proficiency Sample Program Final Report Issued December 2002 Participation: 62 Total Laboratories 2 Laboratories Determined to be Invalid 4 Laboratories Determined to be Outliers 56 Total Laboratories Included in Analysis Sample 189 Sample 190 CV% CV% Average Average (189) (190) 1.304 33.190.423 1.196 31.70 0.461 11.61 11.15 1s d2s 1.334 1.389 0.155 0.438 CV% 1s Reproducibility (Sample 190)Reproducibility (Sample 189) d2s CV% 1s d2s Sa m pl e 19 0 Average Results Graph and Analysis Results for AASHTO T314 / D6723 (Strain) AMRL Performance Graded Binder Samples 189 and 190 AMRL Performance Graded Binder Samples 189 and 190 Determining the Fracture Properties of Asphalt Binder in Direct Tension Sample 189 Asphalt Grade: PG 64-22 / AC 30 Repeatability Lines With Small Dash Marks - Sample Outlier Boundaries Lines With Alternating Dash Marks - Sample Medians Line With Large Dash Marks - Center Diagonal Black Hexagon - Data Within is Used for Analysis Graph Legend -1.83 -0.547 0.736 2.019 3.302 -1.79 -0.552 0.686 1.924 3.162
L-6 Source of Data: AASHTO Materials Reference Laboratory Proficiency Sample Program Final Report Issued May 2003 Participation: 59 Total Laboratories 2 Laboratories Determined to be Invalid 8 Laboratories Determined to be Outliers 49 Total Laboratories Included in Analysis Sample 191 Sample 192 CV% CV% Average Average (191) (192) Asphalt Grade: PG 52-34 / AC 10 Repeatability Lines With Small Dash Marks - Sample Outlier Boundaries Lines With Alternating Dash Marks - Sample Medians Line With Large Dash Marks - Center Diagonal Black Hexagon - Data Within is Used for Analysis Graph Legend Sample 191 1s d2s Sa m pl e 19 2 Average Results Graph and Analysis Results for AASHTO T314 / D6723 (Strain) AMRL Performance Graded Binder Samples 191 and 192 AMRL Performance Graded Binder Samples 191 and 192 Determining the Fracture Properties of Asphalt Binder in Direct Tension Reproducibility (Sample 192)Reproducibility (Sample 191) d2s CV% 8.08 8.29 1s d2s 1.386 1.351 0.112 0.317 CV% 1s 0.798 20.890.273 0.772 19.69 0.282 -0.66 0.156 0.972 1.788 2.604 3.42 -0.92 0.008 0.936 1.864 2.792 3.72
L-7 Source of Data: AASHTO Materials Reference Laboratory Proficiency Sample Program Final Report Issued December 2003 Participation: 62 Total Laboratories 0 Laboratories Determined to be Invalid 1 Laboratories Determined to be Outliers 61 Total Laboratories Included in Analysis Sample 193 Sample 194 CV% CV% Average Average (193) (194) Asphalt Grade: PG 64-22 / AC 20 Repeatability Lines With Small Dash Marks - Sample Outlier Boundaries Lines With Alternating Dash Marks - Sample Medians Line With Large Dash Marks - Center Diagonal Black Hexagon - Data Within is Used for Analysis Graph Legend Sample 193 1s d2s Sa m pl e 19 4 Average Results Graph and Analysis Results for AASHTO T314 / D6723 (Strain) AMRL Performance Graded Binder Samples 193 and 194 AMRL Performance Graded Binder Samples 193 and 194 Determining the Fracture Properties of Asphalt Binder in Direct Tension Reproducibility (Sample 194)Reproducibility (Sample 193) d2s CV% 13.23 13.38 1s d2s 2.692 2.660 0.356 1.007 CV% 1s 2.824 37.531.021 2.889 37.94 0.998 -4.43 -1.578 1.274 4.126 6.978 9.83 -3.96 -1.299 1.362 4.023 6.684
L-8 Source of Data: AASHTO Materials Reference Laboratory Proficiency Sample Program Final Report Issued May 2004 Participation: 60 Total Laboratories 2 Laboratories Determined to be Invalid 2 Laboratories Determined to be Outliers 56 Total Laboratories Included in Analysis Sample 195 Sample 196 CV% CV% Average Average (195) (196) 1.146 29.930.391 1.106 28.75 0.405 12.81 12.88 1s d2s 1.360 1.353 0.174 0.493 CV% 1s Reproducibility (Sample 196)Reproducibility (Sample 195) d2s CV% 1s d2s Sa m pl e 19 6 Average Results Graph and Analysis Results for AASHTO T314 / D6723 (Strain) AMRL Performance Graded Binder Samples 195 and 196 AMRL Performance Graded Binder Samples 195 and 196 Determining the Fracture Properties of Asphalt Binder in Direct Tension Sample 195 Asphalt Grade: PG 70-22 / -- Repeatability Lines With Small Dash Marks - Sample Outlier Boundaries Lines With Alternating Dash Marks - Sample Medians Line With Large Dash Marks - Center Diagonal Black Hexagon - Data Within is Used for Analysis Graph Legend -1.16 -0.128 0.904 1.936 2.968 -1.46 -0.308 0.844 1.996 3.148