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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
×
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
×
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Suggested Citation:"APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES." National Academies of Sciences, Engineering, and Medicine. 2021. Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures. Washington, DC: The National Academies Press. doi: 10.17226/26302.
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183 APPENDIX E: LABORATORY TEST DATA SUMMARY TABLES MIXTURE TEST DATA Table E-1. Bending Beam Fatigue Test Data at 20°C. Binder Code Air Voids (%) Micro-strain Initial Stiffness (MPa) Fatigue Cycles A 6.8 1300 2,111 33,400 7.9 1300 1,717 106,332 6.0 1200 2,216 67,413 6.4 1000 2,384 147,910 6.9 800 2,823 243,594 7.9 700 2,376 1,839,006 7.0 700 2,552 4,663,908 B 7.2 600 6,876 12,882 7.5 500 6,712 73,493 6.6 500 8,424 117,489 6.7 400 6,984 197,242 7.0 400 7,535 258,027 7.4 300 6,595 9,172,759 C 6.7 1200 2,238 103,117 7.5 1200 2,027 68,984 7.1 1000 2,200 129,817 6.1 800 2,800 404,265 6.1 700 2,636 1,547,331 6.9 700 2,832 1,090,184 I 7.7 700 4,801 35,995 7.4 700 4,842 37,692 6.7 700 4,484 41,686 7.4 400 5,156 1,024,275 7.5 400 5,135 761,494 7.7 400 5,151 1,079,775 J 6.4 900 4,522 45,972 6.8 900 4,575 35,789 6.3 900 4,620 36,307 5.4 700 4,928 118,394 6.2 500 4,535 1,562,248 6.7 500 4,947 2,249,486 7.2 500 4,930 643,181 K 8.3 800 4,279 41,807 7.9 800 4,324 37,800 7.0 800 4,769 18,999

184 Binder Code Air Voids (%) Micro-strain Initial Stiffness (MPa) Fatigue Cycles 6.8 800 4,747 35,075 6.9 400 5,722 1,496,235 7.2 400 5,204 2,791,472 6.5 400 5,408 2,405,747 M 6.3 1300 2,103 96,605 6.9 1300 2,118 50,118 7.0 1300 1,950 75,422 6.5 1000 2,152 248,313 6.9 900 1,990 310,217 7.4 800 2,199 1,379,060 O 6.3 1000 5,495 12,196 6.0 1000 6,134 14,412 7.3 1000 5,232 8,128 6.3 500 6,439 844,630 6.0 500 6,429 683,911 6.4 500 6,738 1,320,788 P 7.6 700 5,734 7,542 6.9 500 6,791 12,919 7.3 500 6,731 17,885 6.7 300 7,288 870,963 7.1 300 6,864 1,865,663 6.8 300 7,935 724,435

185 Table E-2. Bending Beam Fatigue Test Data at 10°C Binder Code Air Voids (%) Micro-strain Initial Stiffness (MPa) Fatigue Cycle A 6.5 300 10,799 727,221 7.7 1000 4,676 4,623 6.8 900 5,041 8,912 6.7 900 4,933 7,585 7.2 800 4,563 11,988 6.5 600 5,774 47,315 6.5 600 5,768 19,109 6.8 400 6,123 591,107 6.8 400 6,321 755,672 B 7.0 500 9,143 6,594 7.0 400 10,383 144,543 7.8 400 12,329 129,817 7.0 300 9,225 176,468 6.9 300 10,048 264,038 7.4 300 10,091 407,380 C 6.0 700 6,434 78,072 7.0 700 6,532 29,427 6.0 700 6,784 33,304 6.3 500 6,498 670,913 6.9 500 6,304 255,074 6.2 400 6,583 6,715,577 I 7.6 600 8,163 18,460 7.3 600 7,774 23,850 7.3 600 6,903 64,379 7.1 400 7,873 159,098 7.3 350 8,472 653,130 7.3 350 8,377 358,921 J 7.2 700 8,045 12,022 6.4 600 7,804 18,620 6.4 600 8,382 24,759 6.8 400 7,812 121,618 7.0 300 7,744 2,293,066 6.3 300 8,332 3,301,794 K 6.7 600 8,933 18,674 6.8 600 9,364 7,943 7.3 600 8,981 17,478 7.7 500 8,620 61,129 7.1 400 8,393 331,131

186 Binder Code Air Voids (%) Micro-strain Initial Stiffness (MPa) Fatigue Cycle 7.7 400 9,087 103,117 7.3 400 9,505 92,789 7.0 300 9,375 4,000,214 7.7 500 8,620 61,129 M 6.9 700 4,960 38,128 7.6 700 4,128 245,470 7.3 700 4,658 257,039 6.5 500 5,311 386,070 7.3 500 4,212 1,957,341 6.8 500 5,132 1,703,138 6.6 400 5,482 8,785,166 O 7.6 800 8,747 16,453 6.9 800 9,240 6,985 7.0 600 9,916 24,126 6.8 600 9,786 50,118 5.8 400 9,767 271,227 7.1 350 10,137 2,686,375 7.8 300 9,574 11,953,635 P 6.6 450 9,494 6,456 6.9 450 8,904 9,278 7.4 400 8,945 69,783 6.6 300 9,386 560,187 7.1 300 11,485 841,395 6.5 300 10,799 727,221

187 Table E-3. Uniaxial Fatigue Test Data Binder Code Testing Temperature Air Voids (%) Nf GR A 6°C 6.8 3.9E+04 2.4E+01 7.1 2.3E+03 1.3E+03 6.8 2.5E+03 1.1E+03 12°C 7.0 3.5E+04 3.4E+01 6.7 1.9E+03 2.7E+03 6.8 1.3E+04 3.2E+02 18°C 6.8 1.6E+04 7.9E+01 6.8 8.7E+03 3.7E+02 7.0 5.4E+03 9.8E+02 7.1 1.8E+04 1.0E+02 B 21°C 7.5 4.1E+03 8.0E+02 7.4 9.3E+03 2.1E+02 27°C 7.6 1.6E+04 9.8E+01 7.3 4.2E+03 6.4E+02 7.4 2.1E+03 1.5E+03 C 9°C 7.6 1.1E+04 2.0E+02 7.2 4.4E+03 4.6E+02 7.1 2.7E+04 2.4E+01 15°C 6.8 1.4E+04 3.6E+02 6.9 6.1E+03 8.5E+02 7.1 1.4E+03 3.9E+03 D 12°C 7.6 2.3E+03 1.4E+03 7.4 8.4E+03 1.9E+02 7.0 5.0E+04 1.5E+01 18°C 7.2 3.8E+03 4.1E+02 7.2 1.9E+04 5.1E+01 7.3 2.5E+03 1.3E+03 E 24°C 6.7 6.9E+03 4.9E+02 7.2 5.5E+04 2.1E+01 7.3 1.1E+04 1.4E+02 30°C 6.5 9.2E+04 1.5E+01 7.4 2.0E+04 7.6E+01 6.6 7.8E+03 2.5E+02 F 19.5°C 7.4 1.7E+03 1.4E+03 7.2 4.1E+03 3.5E+02 6.9 5.5E+04 1.2E+01 25.5°C 6.8 1.1E+04 1.0E+02 7.2 3.4E+03 5.5E+02 7.0 5.0E+04 1.7E+01 G 30°C 6.5 9.3E+04 1.1E+01 6.7 3.7E+03 5.1E+02

188 7.2 1.1E+04 1.8E+02 6.9 4.4E+03 4.4E+02 36°C 6.6 1.8E+04 9.3E+01 6.9 7.1E+04 1.1E+01 7.1 2.0E+04 7.7E+01 7.1 1.2E+04 1.6E+02 H 21°C 7.1 7.6E+03 1.6E+02 7.3 5.2E+04 3.4E+01 7.1 1.7E+03 2.5E+03 27°C 7.3 1.7E+04 1.1E+02 7.5 1.2E+04 2.6E+02 7.3 8.9E+03 4.5E+02 I 12°C 6.5 4.1E+03 7.8E+02 7.1 1.5E+04 7.6E+01 18°C 6.9 8.9E+03 1.4E+02 7.0 3.0E+03 9.2E+02 6.8 4.0E+04 2.8E+01 7.5 1.5E+04 9.6E+01 J 15°C 7.1 9.4E+03 1.8E+02 7.3 3.2E+03 1.1E+03 7.1 8.6E+04 1.4E+01 21°C 7.3 9.6E+03 3.0E+02 7.2 4.7E+03 1.1E+03 7.1 1.1E+04 2.0E+02 K 12°C 6.5 2.8E+04 3.6E+01 6.9 7.0E+03 2.3E+02 6.8 1.5E+03 1.4E+03 7.3 5.9E+03 1.8E+02 18°C 6.5 2.0E+03 1.9E+03 6.5 1.3E+04 1.4E+02 6.5 5.1E+04 2.5E+01 24°C 7.2 1.5E+04 1.4E+02 7.1 3.9E+03 8.2E+02 7.0 1.9E+03 1.8E+03 L 27°C 7.2 3.2E+03 5.9E+02 6.9 2.5E+03 4.3E+02 33°C 7.2 1.8E+03 8.0E+02 7.2 5.7E+03 1.4E+02 7.1 7.5E+04 4.5E+00 M 24°C 6.7 1.2E+05 5.9E+00 6.5 3.5E+04 3.6E+01 6.5 1.2E+04 1.4E+02 30°C 6.9 5.5E+03 3.7E+02 7.1 1.8E+03 1.7E+03 N 21°C 6.5 2.3E+05 4.2E+00

189 6.5 8.1E+04 2.5E+01 6.5 9.0E+03 4.5E+02 27°C 6.7 1.2E+05 5.2E+00 7.6 2.1E+05 3.9E+00 7.0 1.3E+04 1.5E+02 O 15°C 6.7 5.2E+04 2.6E+01 6.7 3.6E+03 1.5E+03 6.7 3.7E+03 4.4E+02 21°C 6.9 5.3E+04 1.1E+01 6.6 2.6E+04 7.4E+01 6.5 2.0E+04 1.3E+02 6.8 7.3E+03 4.2E+02 27°C 6.7 1.7E+04 7.8E+01 6.6 4.2E+03 7.3E+02 P 21°C 7.5 1.2E+03 3.5E+03 7.3 1.9E+03 1.2E+03 7.7 1.2E+04 8.1E+01 27°C 7.3 9.9E+03 3.3E+02 7.6 1.1E+03 3.4E+03 7.4 1.3E+04 7.6E+01

190 BINDER TEST DATA Table E-4. DSR Frequency Sweeps Binder: A B C D Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 10 0.1 3.18E+06 36.2 8.76E+06 35.9 1.21E+06 45.2 4.16E+06 48.4 10 0.158 3.83E+06 35 1.06E+07 34.9 1.54E+06 44.4 5.39E+06 46.6 10 0.251 4.58E+06 33.9 1.27E+07 34.1 1.93E+06 43.8 6.82E+06 45 10 0.398 5.43E+06 33 1.51E+07 33.3 2.42E+06 43.1 8.56E+06 43.4 10 0.631 6.41E+06 32.1 1.78E+07 32.5 3.02E+06 42.5 1.07E+07 41.8 10 1 7.53E+06 31.2 2.10E+07 31.8 3.74E+06 41.8 1.32E+07 40.3 10 1.58 8.82E+06 30.5 2.47E+07 31.1 4.64E+06 41.2 1.62E+07 38.9 10 2.51 1.03E+07 29.9 2.90E+07 30.4 5.72E+06 40.6 1.97E+07 37.5 10 3.98 1.19E+07 29.3 3.38E+07 29.7 7.04E+06 39.9 2.38E+07 36.2 10 6.31 1.38E+07 28.7 3.93E+07 29.1 8.61E+06 39.3 2.86E+07 35 10 10 1.60E+07 28.3 4.55E+07 28.5 1.05E+07 38.7 3.40E+07 33.8 10 15.8 1.85E+07 27.8 5.26E+07 27.8 1.28E+07 38.1 4.04E+07 32.7 10 25.1 2.13E+07 27.4 6.06E+07 27.2 1.56E+07 37.5 4.76E+07 31.5 10 39.8 2.44E+07 27.1 6.96E+07 26.5 1.88E+07 36.9 5.58E+07 30.5 10 63.1 2.79E+07 26.7 7.96E+07 25.9 2.27E+07 36.2 6.49E+07 29.4 10 100 3.19E+07 26.4 9.08E+07 25.2 2.73E+07 35.6 7.51E+07 28.4 22 0.1 6.48E+05 44.7 1.79E+06 42 2.05E+05 48.2 4.68E+05 60.7 22 0.158 8.09E+05 43.3 2.22E+06 41.1 2.63E+05 47.9 6.35E+05 59.1 22 0.251 1.00E+06 42.1 2.73E+06 40.3 3.36E+05 47.7 8.56E+05 57.7 22 0.398 1.23E+06 41 3.35E+06 39.6 4.29E+05 47.4 1.15E+06 56.2 22 0.631 1.51E+06 39.9 4.08E+06 38.9 5.47E+05 47.1 1.52E+06 54.7 22 1 1.85E+06 38.9 4.97E+06 38.2 6.96E+05 46.8 2.01E+06 53.1 22 1.58 2.25E+06 37.9 6.03E+06 37.6 8.84E+05 46.4 2.62E+06 51.6 22 2.51 2.72E+06 37.1 7.29E+06 36.9 1.12E+06 46.1 3.40E+06 50.2 22 3.98 3.27E+06 36.3 8.78E+06 36.4 1.42E+06 45.8 4.36E+06 48.8 22 6.31 3.92E+06 35.6 1.06E+07 35.8 1.79E+06 45.4 5.58E+06 47.3 22 10 4.68E+06 34.9 1.26E+07 35.2 2.26E+06 45 7.07E+06 46 22 15.8 5.57E+06 34.3 1.51E+07 34.7 2.84E+06 44.6 8.87E+06 44.6 22 25.1 6.60E+06 33.7 1.80E+07 34.1 3.55E+06 44.1 1.11E+07 43.3 22 39.8 7.82E+06 33.2 2.13E+07 33.6 4.44E+06 43.6 1.38E+07 42 22 63.1 9.22E+06 32.6 2.52E+07 33 5.55E+06 42.7 1.70E+07 40.7 22 100 1.09E+07 32.4 2.98E+07 32.4 6.94E+06 42.7 2.08E+07 39.5

191 Table E-4. DSR Frequency Sweeps (continued). Binder: A B C D Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 34 0.1 9.89E+04 54.2 3.22E+05 47.4 3.67E+04 49.8 4.16E+04 71.2 34 0.158 1.30E+05 52.7 4.10E+05 46.6 4.74E+04 49.7 5.95E+04 69.7 34 0.251 1.70E+05 51.3 5.18E+05 45.9 6.11E+04 49.7 8.47E+04 68.4 34 0.398 2.19E+05 50 6.53E+05 45.3 7.87E+04 49.7 1.20E+05 67.1 34 0.631 2.81E+05 48.7 8.21E+05 44.7 1.01E+05 49.7 1.68E+05 65.7 34 1 3.59E+05 47.6 1.03E+06 44.1 1.31E+05 49.7 2.34E+05 64.4 34 1.58 4.56E+05 46.5 1.29E+06 43.5 1.69E+05 49.6 3.24E+05 63.1 34 2.51 5.75E+05 45.5 1.60E+06 43 2.18E+05 49.6 4.46E+05 61.8 34 3.98 7.21E+05 44.5 1.99E+06 42.6 2.81E+05 49.6 6.12E+05 60.5 34 6.31 9.00E+05 43.7 2.46E+06 42.1 3.62E+05 49.6 8.31E+05 59.3 34 10 1.12E+06 42.9 3.04E+06 41.6 4.66E+05 49.6 1.12E+06 58 34 15.8 1.38E+06 42.1 3.74E+06 41.2 6.00E+05 49.5 1.49E+06 56.7 34 25.1 1.70E+06 41.4 4.59E+06 40.7 7.73E+05 49.4 1.98E+06 55.3 34 39.8 2.09E+06 40.8 5.62E+06 40.2 9.95E+05 49.3 2.61E+06 53.8 34 63.1 2.55E+06 40.3 6.88E+06 39.5 1.28E+06 49.2 3.43E+06 52.8 34 100 3.10E+06 39.9 8.40E+06 39.5 1.64E+06 49.2 4.46E+06 51.6 46 0.1 13700 64.9 50600 53.5 5890 55.4 3450 81.1 46 0.158 19200 62.9 66100 52 7830 54.7 5250 79.7 46 0.251 26400 61.2 85700 51.3 10300 54.1 7880 78.3 46 0.398 36000 59.6 111000 50.6 13600 53.7 11700 76.9 46 0.631 48700 58 144000 49.9 17800 53.2 17300 75.5 46 1 65200 56.6 185000 49.5 23300 53 25400 74.1 46 1.58 86900 55.3 238000 49 30600 52.8 37000 72.7 46 2.51 115000 54.1 306000 48.6 40000 52.7 53400 71.5 46 3.98 151000 53 392000 48.3 52300 52.7 76800 70.2 46 6.31 197000 51.9 501000 48 68500 52.8 110000 69 46 10 256000 51 640000 47.8 89700 53 155000 67.9 46 15.8 331000 50.1 816000 47.6 118000 53.1 219000 66.8 46 25.1 427000 49.3 1040000 47.4 155000 53.3 308000 65.7 46 39.8 547000 48.5 1320000 47.2 203000 53.5 430000 64.6 46 63.1 700000 47.9 1690000 47.1 267000 53.6 596000 63.5 46 100 892000 47.2 2140000 47 352000 53.8 822000 62.5

192 Table E-4. DSR Frequency Sweeps (continued). Binder: E F G H Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 10 0.1 8.95E+06 31.8 7.57E+06 37.9 7.17E+06 39.9 6.37E+06 35.2 10 0.158 1.06E+07 30.9 9.25E+06 36.6 8.89E+06 38.4 7.69E+06 34.3 10 0.251 1.24E+07 30.2 1.12E+07 35.5 1.08E+07 37.2 9.15E+06 33.4 10 0.398 1.45E+07 29.5 1.34E+07 34.4 1.31E+07 36 1.09E+07 32.6 10 0.631 1.68E+07 28.9 1.59E+07 33.4 1.57E+07 34.8 1.29E+07 31.8 10 1 1.95E+07 28.3 1.89E+07 32.5 1.88E+07 33.7 1.52E+07 31.1 10 1.58 2.25E+07 27.8 2.22E+07 31.6 2.23E+07 32.6 1.78E+07 30.5 10 2.51 2.59E+07 27.3 2.61E+07 30.7 2.63E+07 31.6 2.07E+07 29.9 10 3.98 2.97E+07 26.9 3.04E+07 30 3.08E+07 30.7 2.40E+07 29.4 10 6.31 3.41E+07 26.4 3.54E+07 29.2 3.58E+07 29.8 2.80E+07 28.9 10 10 3.90E+07 26 4.10E+07 28.5 4.17E+07 28.9 3.24E+07 28.4 10 15.8 4.45E+07 25.7 4.74E+07 27.8 4.82E+07 28.1 3.74E+07 27.9 10 25.1 5.07E+07 25.3 5.46E+07 27.1 5.56E+07 27.2 4.31E+07 27.4 10 39.8 5.76E+07 24.9 6.26E+07 26.4 6.37E+07 26.4 4.96E+07 26.9 10 63.1 6.54E+07 24.5 7.15E+07 25.7 7.29E+07 25.6 5.69E+07 26.4 10 100 7.41E+07 24.1 8.15E+07 25 8.29E+07 24.8 6.51E+07 25.9 22 0.1 2.12E+06 37.6 1.41E+06 46.6 1.20E+06 48.6 1.33E+06 41.8 22 0.158 2.56E+06 36.7 1.78E+06 45.3 1.55E+06 47.4 1.64E+06 40.8 22 0.251 3.08E+06 36 2.23E+06 44.1 1.96E+06 46.4 2.02E+06 40 22 0.398 3.69E+06 35.3 2.78E+06 43 2.48E+06 45.3 2.46E+06 39.2 22 0.631 4.40E+06 34.6 3.45E+06 41.9 3.12E+06 44.2 3.00E+06 38.3 22 1 5.24E+06 33.9 4.26E+06 40.8 3.90E+06 43.1 3.64E+06 37.6 22 1.58 6.22E+06 33.3 5.23E+06 39.8 4.85E+06 42.1 4.40E+06 36.9 22 2.51 7.35E+06 32.8 6.38E+06 38.9 5.99E+06 41 5.29E+06 36.3 22 3.98 8.66E+06 32.3 7.76E+06 38 7.37E+06 40 6.35E+06 35.7 22 6.31 1.02E+07 31.9 9.40E+06 37.1 9.00E+06 39 7.59E+06 35.1 22 10 1.20E+07 31.5 1.13E+07 36.3 1.09E+07 38 9.06E+06 34.6 22 15.8 1.40E+07 31.1 1.36E+07 35.5 1.32E+07 37.1 1.08E+07 34.1 22 25.1 1.64E+07 30.7 1.62E+07 34.8 1.59E+07 36.2 1.28E+07 33.6 22 39.8 1.91E+07 30.4 1.93E+07 34 1.91E+07 35.3 1.51E+07 33.2 22 63.1 2.22E+07 30 2.29E+07 33.3 2.27E+07 34.4 1.79E+07 32.8 22 100 2.58E+07 29.7 2.70E+07 32.6 2.70E+07 33.5 2.11E+07 32.3

193 Table E-4. DSR Frequency Sweeps (continued). Binder: E F G H Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 34 0.1 4.30E+05 43.1 1.96E+05 55.7 1.71E+05 53.2 2.20E+05 48.6 34 0.158 5.34E+05 42.3 2.60E+05 54.4 2.24E+05 52.8 2.82E+05 47.7 34 0.251 6.61E+05 41.6 3.41E+05 53.2 2.93E+05 52.4 3.58E+05 46.8 34 0.398 8.13E+05 41 4.46E+05 52 3.83E+05 52 4.53E+05 46.1 34 0.631 9.98E+05 40.3 5.78E+05 50.8 4.99E+05 51.4 5.70E+05 45.3 34 1 1.22E+06 39.7 7.47E+05 49.7 6.50E+05 50.7 7.15E+05 44.5 34 1.58 1.49E+06 39.1 9.59E+05 48.7 8.42E+05 50.1 8.94E+05 43.8 34 2.51 1.81E+06 38.6 1.22E+06 47.7 1.09E+06 49.4 1.11E+06 43.2 34 3.98 2.19E+06 38.1 1.55E+06 46.7 1.40E+06 48.6 1.38E+06 42.6 34 6.31 2.65E+06 37.7 1.96E+06 45.8 1.78E+06 47.9 1.71E+06 42 34 10 3.20E+06 37.3 2.47E+06 45 2.27E+06 47.1 2.11E+06 41.5 34 15.8 3.84E+06 36.9 3.08E+06 44.1 2.87E+06 46.3 2.59E+06 41 34 25.1 4.61E+06 36.5 3.83E+06 43.3 3.60E+06 45.4 3.17E+06 40.5 34 39.8 5.52E+06 36.1 4.75E+06 42.4 4.51E+06 44.4 3.87E+06 40 34 63.1 6.61E+06 35.6 5.87E+06 41.4 5.65E+06 43.3 4.73E+06 39.7 34 100 7.87E+06 35.7 7.22E+06 41.1 7.02E+06 42.9 5.73E+06 39.4 46 0.1 83500 48.2 26700 65.1 25700 53.2 35600 54.2 46 0.158 107000 47.2 37300 63.2 34100 53.4 47000 53.1 46 0.251 137000 46.4 51400 61.7 44800 53.6 61900 52.6 46 0.398 174000 45.8 70200 60.4 58900 53.7 81000 51.8 46 0.631 219000 45.1 94900 59 77600 53.7 105000 51.1 46 1 275000 44.5 128000 57.8 102000 53.7 136000 50.5 46 1.58 345000 43.9 171000 56.6 135000 53.8 176000 49.8 46 2.51 431000 43.4 228000 55.6 178000 53.8 227000 49.2 46 3.98 538000 42.9 303000 54.6 235000 53.7 292000 48.7 46 6.31 669000 42.5 399000 53.8 310000 53.6 374000 48.2 46 10 830000 42.1 523000 52.9 408000 53.5 478000 47.7 46 15.8 1030000 41.8 684000 52.1 537000 53.2 610000 47.3 46 25.1 1270000 41.4 891000 51.4 705000 52.9 775000 46.9 46 39.8 1570000 41.2 1160000 50.7 924000 52.6 984000 46.5 46 63.1 1940000 40.9 1490000 50.1 1210000 52.2 1250000 46.2 46 100 2380000 40.7 1930000 49.6 1580000 51.8 1580000 46

194 Table E-4. DSR Frequency Sweeps (continued). Binder: I J K L Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 10 0.1 2.98E+06 48.9 2.35E+06 44.8 6.99E+06 37.8 1.40E+07 30 10 0.158 3.85E+06 47.4 2.97E+06 43.6 8.53E+06 36.4 1.64E+07 29 10 0.251 4.90E+06 46 3.72E+06 42.6 1.03E+07 35.2 1.90E+07 28.2 10 0.398 6.18E+06 44.7 4.63E+06 41.6 1.23E+07 34 2.19E+07 27.4 10 0.631 7.75E+06 43.3 5.71E+06 40.6 1.46E+07 32.9 2.52E+07 26.7 10 1 9.64E+06 42 7.02E+06 39.6 1.73E+07 32 2.88E+07 26 10 1.58 1.19E+07 40.7 8.59E+06 38.6 2.03E+07 31 3.29E+07 25.4 10 2.51 1.46E+07 39.5 1.04E+07 37.7 2.37E+07 30.2 3.74E+07 24.9 10 3.98 1.79E+07 38.3 1.26E+07 36.8 2.76E+07 29.4 4.23E+07 24.4 10 6.31 2.17E+07 37.2 1.52E+07 36 3.19E+07 28.7 4.80E+07 23.9 10 10 2.61E+07 36.1 1.82E+07 35.1 3.68E+07 28 5.41E+07 23.4 10 15.8 3.14E+07 35 2.18E+07 34.3 4.24E+07 27.3 6.10E+07 23 10 25.1 3.74E+07 33.9 2.59E+07 33.5 4.86E+07 26.6 6.85E+07 22.6 10 39.8 4.43E+07 32.8 3.07E+07 32.7 5.58E+07 26 7.68E+07 22.2 10 63.1 5.24E+07 31.8 3.62E+07 31.9 6.38E+07 25.3 8.59E+07 21.8 10 100 6.14E+07 30.7 4.26E+07 31.1 7.25E+07 24.7 9.59E+07 21.4 22 0.1 3.42E+05 58.6 3.61E+05 50.1 1.31E+06 47 3.71E+06 36 22 0.158 4.61E+05 57.3 4.65E+05 49.6 1.67E+06 45.6 4.46E+06 35 22 0.251 6.16E+05 56.2 5.98E+05 49.1 2.09E+06 44.3 5.31E+06 34 22 0.398 8.18E+05 55.2 7.67E+05 48.6 2.61E+06 43.1 6.29E+06 33.2 22 0.631 1.08E+06 54 9.82E+05 47.9 3.24E+06 41.9 7.43E+06 32.4 22 1 1.42E+06 52.8 1.25E+06 47.3 4.00E+06 40.7 8.74E+06 31.7 22 1.58 1.86E+06 51.7 1.59E+06 46.6 4.90E+06 39.6 1.03E+07 31 22 2.51 2.41E+06 50.5 2.02E+06 45.9 5.98E+06 38.6 1.20E+07 30.3 22 3.98 3.12E+06 49.4 2.55E+06 45.1 7.25E+06 37.7 1.39E+07 29.8 22 6.31 4.00E+06 48.3 3.21E+06 44.4 8.75E+06 36.8 1.62E+07 29.2 22 10 5.10E+06 47.1 4.01E+06 43.6 1.05E+07 35.9 1.87E+07 28.7 22 15.8 6.46E+06 46 5.00E+06 42.9 1.26E+07 35.1 2.16E+07 28.2 22 25.1 8.12E+06 44.8 6.19E+06 42.1 1.50E+07 34.3 2.49E+07 27.8 22 39.8 1.02E+07 43.7 7.68E+06 41.3 1.78E+07 33.5 2.86E+07 27.4 22 63.1 1.27E+07 42.6 9.45E+06 40.5 2.10E+07 32.8 3.28E+07 27 22 100 1.57E+07 41.4 1.16E+07 39.3 2.48E+07 32.1 3.75E+07 26.6

195 Table E-4. DSR Frequency Sweeps (continued). Binder: I J K L Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 34 0.1 3.59E+04 67.4 5.61E+04 51.3 1.76E+05 56.9 8.00E+05 42.5 34 0.158 5.05E+04 66 7.30E+04 51.2 2.35E+05 55.4 9.92E+05 41.5 34 0.251 7.05E+04 64.7 9.49E+04 51.3 3.10E+05 54 1.22E+06 40.5 34 0.398 9.78E+04 63.6 1.23E+05 51.3 4.07E+05 52.8 1.49E+06 39.7 34 0.631 1.35E+05 62.5 1.60E+05 51.2 5.30E+05 51.5 1.82E+06 38.8 34 1 1.85E+05 61.4 2.08E+05 51.2 6.86E+05 50.3 2.21E+06 38 34 1.58 2.52E+05 60.4 2.71E+05 51.1 8.85E+05 49.1 2.67E+06 37.3 34 2.51 3.42E+05 59.5 3.52E+05 50.9 1.13E+06 48.1 3.21E+06 36.6 34 3.98 4.63E+05 58.6 4.57E+05 50.7 1.44E+06 47 3.85E+06 36 34 6.31 6.24E+05 57.7 5.92E+05 50.5 1.82E+06 46 4.61E+06 35.4 34 10 8.35E+05 56.7 7.66E+05 50.2 2.29E+06 45.1 5.49E+06 34.8 34 15.8 1.11E+06 55.8 9.88E+05 49.8 2.86E+06 44.2 6.52E+06 34.3 34 25.1 1.47E+06 54.8 1.27E+06 49.3 3.56E+06 43.3 7.70E+06 33.8 34 39.8 1.95E+06 53.8 1.64E+06 49 4.41E+06 42.3 9.11E+06 33.4 34 63.1 2.55E+06 52.9 2.10E+06 48.5 5.45E+06 41.2 1.07E+07 32.8 34 100 3.33E+06 51.9 2.68E+06 48 6.69E+06 40.9 1.26E+07 32.5 46 0.1 3960 77.9 10300 52.9 23000 67.1 128000 49.3 46 0.158 5920 76.1 13500 52.6 32500 65 165000 48.2 46 0.251 8720 74.5 17600 52.6 44900 63.7 211000 47 46 0.398 12700 73 23100 52.4 62200 61.9 268000 45.8 46 0.631 18400 71.4 30100 52.6 84600 60.6 338000 45.2 46 1 26300 70 39400 52.5 115000 59.2 425000 44.4 46 1.58 37500 68.6 51600 52.8 155000 57.9 533000 43.8 46 2.51 53000 67.4 67500 53 208000 56.8 665000 43.1 46 3.98 74500 66.3 88700 53.2 276000 55.7 827000 42.6 46 6.31 104000 65.3 116000 53.5 366000 54.7 1030000 42.1 46 10 145000 64.4 153000 53.7 483000 53.7 1270000 41.7 46 15.8 201000 63.6 202000 53.9 633000 52.9 1570000 41.3 46 25.1 278000 62.8 267000 54.1 827000 52 1940000 41 46 39.8 382000 62.1 352000 54.2 1080000 51.3 2380000 40.7 46 63.1 523000 61.4 465000 54.2 1390000 50.6 2930000 40.5 46 100 715000 60.7 615000 54.2 1800000 50 3590000 40.4

196 Table E-4. DSR Frequency Sweeps (continued). Binder: M N O P Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 10 0.1 1.92E+06 34.5 1.74E+06 33.1 6.71E+06 39.6 1.01E+07 35.4 10 0.158 2.32E+06 34.2 2.08E+06 32.3 8.31E+06 38.4 1.22E+07 34.2 10 0.251 2.77E+06 34 2.45E+06 31.6 1.02E+07 37.3 1.45E+07 33.2 10 0.398 3.30E+06 33.8 2.89E+06 31.1 1.23E+07 36.3 1.72E+07 32.2 10 0.631 3.93E+06 33.5 3.38E+06 30.6 1.48E+07 35.3 2.02E+07 31.3 10 1 4.67E+06 33.3 3.95E+06 30.2 1.77E+07 34.4 2.37E+07 30.4 10 1.58 5.54E+06 33 4.61E+06 29.8 2.11E+07 33.5 2.76E+07 29.6 10 2.51 6.56E+06 32.8 5.36E+06 29.5 2.49E+07 32.6 3.21E+07 28.9 10 3.98 7.76E+06 32.6 6.23E+06 29.3 2.94E+07 31.8 3.71E+07 28.1 10 6.31 9.17E+06 32.3 7.23E+06 29.1 3.46E+07 31 4.28E+07 27.4 10 10 1.08E+07 32.1 8.38E+06 29 4.05E+07 30.1 4.92E+07 26.8 10 15.8 1.27E+07 31.9 9.71E+06 28.9 4.71E+07 29.3 5.63E+07 26.1 10 25.1 1.50E+07 31.6 1.13E+07 28.9 5.47E+07 28.5 6.43E+07 25.5 10 39.8 1.76E+07 31.3 1.30E+07 28.9 6.32E+07 27.7 7.31E+07 24.9 10 63.1 2.07E+07 31.1 1.51E+07 28.9 7.27E+07 26.9 8.29E+07 24.2 10 100 2.43E+07 30.7 1.76E+07 28.6 8.32E+07 26 9.37E+07 23.6 22 0.1 5.20E+05 33.1 4.40E+05 36.9 1.18E+06 46.6 2.08E+06 43 22 0.158 6.17E+05 33.3 5.32E+05 36.2 1.50E+06 45.8 2.58E+06 41.9 22 0.251 7.31E+05 33.6 6.39E+05 35.7 1.88E+06 45 3.18E+06 40.9 22 0.398 8.67E+05 33.8 7.65E+05 35.2 2.35E+06 44.2 3.90E+06 39.9 22 0.631 1.03E+06 34 9.13E+05 34.7 2.94E+06 43.4 4.76E+06 38.9 22 1 1.23E+06 34.2 1.09E+06 34.3 3.66E+06 42.5 5.79E+06 38 22 1.58 1.46E+06 34.4 1.29E+06 33.9 4.54E+06 41.7 7.02E+06 37.1 22 2.51 1.74E+06 34.6 1.53E+06 33.6 5.60E+06 40.9 8.45E+06 36.3 22 3.98 2.08E+06 34.8 1.81E+06 33.3 6.88E+06 40.1 1.02E+07 35.5 22 6.31 2.48E+06 35 2.15E+06 33.1 8.42E+06 39.4 1.21E+07 34.7 22 10 2.96E+06 35.1 2.53E+06 33 1.03E+07 38.6 1.44E+07 34 22 15.8 3.54E+06 35.2 2.99E+06 32.8 1.24E+07 37.8 1.71E+07 33.3 22 25.1 4.23E+06 35.3 3.52E+06 32.8 1.51E+07 37.1 2.02E+07 32.6 22 39.8 5.06E+06 35.3 4.15E+06 32.6 1.81E+07 36.3 2.38E+07 32 22 63.1 6.07E+06 35 4.91E+06 32.8 2.18E+07 35.5 2.79E+07 31.3 22 100 7.27E+06 35.4 5.78E+06 32.9 2.60E+07 34.7 3.26E+07 30.7

197 Table E-4. DSR Frequency Sweeps (continued). Binder: M N O P Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 34 0.1 1.57E+05 29.9 9.83E+04 39.2 1.76E+05 51.2 3.40E+05 50.2 34 0.158 1.83E+05 30.3 1.20E+05 38.8 2.28E+05 50.7 4.38E+05 49.1 34 0.251 2.13E+05 30.7 1.46E+05 38.4 2.96E+05 50.3 5.61E+05 48.2 34 0.398 2.48E+05 31.2 1.78E+05 38.2 3.82E+05 50 7.15E+05 47.3 34 0.631 2.91E+05 31.7 2.15E+05 37.9 4.93E+05 49.5 9.06E+05 46.4 34 1 3.42E+05 32.2 2.61E+05 37.7 6.34E+05 49 1.15E+06 45.6 34 1.58 4.03E+05 32.8 3.15E+05 37.5 8.14E+05 48.5 1.44E+06 44.7 34 2.51 4.75E+05 33.4 3.80E+05 37.4 1.04E+06 48 1.80E+06 44 34 3.98 5.63E+05 34.1 4.59E+05 37.3 1.33E+06 47.5 2.25E+06 43.2 34 6.31 6.70E+05 34.7 5.53E+05 37.2 1.69E+06 47 2.79E+06 42.5 34 10 7.99E+05 35.4 6.65E+05 37.2 2.14E+06 46.4 3.46E+06 41.8 34 15.8 9.55E+05 36 8.00E+05 37.2 2.70E+06 45.9 4.25E+06 41.1 34 25.1 1.15E+06 36.6 9.63E+05 37.1 3.39E+06 45.2 5.21E+06 40.4 34 39.8 1.38E+06 37.3 1.16E+06 37.4 4.25E+06 44.5 6.36E+06 39.7 34 63.1 1.66E+06 37.9 1.39E+06 37.6 5.32E+06 43.5 7.75E+06 38.8 34 100 2.01E+06 38.5 1.66E+06 37.9 6.62E+06 43.4 9.42E+06 38.5 46 0.1 45600 25.5 25500 39.5 32200 53.1 47900 59 46 0.158 52200 25.8 31500 39.4 42400 52.7 65200 57.7 46 0.251 59800 26.3 38700 39.2 55500 52.5 86600 56.6 46 0.398 68400 27.1 47300 38.9 72600 52.4 115000 55.3 46 0.631 78300 27.7 57800 38.9 94800 52.2 152000 54.2 46 1 90200 28.3 70600 39 124000 52.1 199000 53.4 46 1.58 104000 29.1 86300 39.1 162000 51.9 260000 52.5 46 2.51 121000 30.1 105000 39.1 211000 51.8 339000 51.8 46 3.98 142000 31.1 129000 39.3 276000 51.7 439000 51.1 46 6.31 166000 32.2 158000 39.4 359000 51.5 566000 50.6 46 10 197000 33.4 193000 39.6 467000 51.3 728000 50 46 15.8 234000 34.6 236000 39.8 607000 51 935000 49.5 46 25.1 280000 35.8 290000 40 789000 50.8 1200000 49 46 39.8 337000 37 356000 40.2 1020000 50.5 1530000 48.6 46 63.1 409000 38.3 437000 40.5 1320000 50.1 1960000 48.2 46 100 500000 39.5 538000 40.8 1700000 49.8 2500000 47.8

198 Table E-4. DSR Frequency Sweeps (continued). Binder: AAA-1 AAB-1 AAC-1 AAD-1 Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 10 0.1 2.56E+05 67 1.12E+06 57.1 1.69E+06 58.9 5.31E+05 59.1 10 0.158 3.61E+05 65.7 1.46E+06 55.4 2.36E+06 56.4 7.20E+05 58.3 10 0.251 5.16E+05 64.6 1.93E+06 53.9 3.17E+06 54.2 9.93E+05 57.4 10 0.398 7.41E+05 63.4 2.51E+06 52.4 4.19E+06 52.1 1.33E+06 56.6 10 0.631 1.04E+06 62 3.28E+06 50.7 5.43E+06 50 1.78E+06 55.6 10 1 1.42E+06 60.7 4.25E+06 49.1 6.99E+06 48 2.37E+06 54.5 10 1.58 1.94E+06 59.3 5.43E+06 47.5 8.89E+06 46.1 3.11E+06 53.4 10 2.51 2.64E+06 57.8 6.88E+06 45.9 1.12E+07 44.2 4.06E+06 52.3 10 3.98 3.54E+06 56.4 8.69E+06 44.4 1.40E+07 42.5 5.31E+06 51.1 10 6.31 4.72E+06 54.8 1.09E+07 43 1.74E+07 40.8 6.93E+06 49.8 10 10 6.24E+06 53.3 1.35E+07 41.6 2.13E+07 39.3 8.88E+06 48.4 10 15.8 8.17E+06 51.7 1.67E+07 40.2 2.60E+07 37.8 1.13E+07 47.1 10 25.1 1.06E+07 50 2.05E+07 38.8 3.14E+07 36.4 1.44E+07 45.7 10 39.8 1.37E+07 48.4 2.50E+07 37.6 3.77E+07 35 1.83E+07 44.2 10 63.1 1.75E+07 46.7 3.01E+07 36.3 4.49E+07 33.7 2.28E+07 42.8 10 100 2.21E+07 45.1 3.61E+07 35.1 5.31E+07 32.4 2.82E+07 41.4 22 0.1 2.21E+04 75.1 1.03E+05 67.6 1.23E+05 71.6 5.87E+04 63.5 22 0.158 3.25E+04 73.8 1.45E+05 66.3 1.79E+05 70.1 8.11E+04 63 22 0.251 4.73E+04 72.7 2.04E+05 65 2.57E+05 68.8 1.12E+05 62.5 22 0.398 6.82E+04 71.6 2.83E+05 63.8 3.65E+05 67.3 1.53E+05 62.1 22 0.631 9.74E+04 70.6 3.91E+05 62.4 5.14E+05 65.6 2.10E+05 61.5 22 1 1.39E+05 69.6 5.38E+05 61 7.16E+05 63.9 2.88E+05 61 22 1.58 1.98E+05 68.6 7.35E+05 59.5 9.91E+05 62.1 3.94E+05 60.4 22 2.51 2.80E+05 67.6 9.94E+05 58.1 1.35E+06 60.3 5.35E+05 59.9 22 3.98 3.95E+05 66.6 1.34E+06 56.7 1.83E+06 58.4 7.27E+05 59.3 22 6.31 5.54E+05 65.6 1.78E+06 55.3 2.46E+06 56.6 9.84E+05 58.6 22 10 7.74E+05 64.6 2.35E+06 53.8 3.26E+06 54.7 1.33E+06 57.8 22 15.8 1.08E+06 63.5 3.07E+06 52.4 4.29E+06 52.9 1.78E+06 57 22 25.1 1.48E+06 62.3 3.99E+06 51 5.57E+06 51.1 2.37E+06 56 22 39.8 2.04E+06 61 5.15E+06 49.5 7.21E+06 49.4 3.15E+06 54.9 22 63.1 2.78E+06 59.7 6.59E+06 47.8 9.22E+06 47.8 4.19E+06 53.8 22 100 3.76E+06 58.4 8.44E+06 46.8 1.17E+07 45.7 5.52E+06 52.8

199 Table E-4. DSR Frequency Sweeps (continued). Binder: AAA-1 AAB-1 AAC-1 AAD-1 Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 34 0.1 2.01E+03 83.1 7880 77.2 6.73E+03 80.5 6.56E+03 71.8 34 0.158 3.09E+03 81.9 11600 76.3 1.03E+04 79.8 9.42E+03 70.9 34 0.251 4.71E+03 80.8 17100 75.2 1.52E+04 79 1.34E+04 69.9 34 0.398 7.10E+03 79.6 25100 74 2.25E+04 78.1 1.91E+04 68.9 34 0.631 1.07E+04 78.3 36900 72.5 3.32E+04 77 2.71E+04 67.8 34 1 1.59E+04 77.1 54100 71.1 4.91E+04 75.8 3.82E+04 66.9 34 1.58 2.37E+04 75.9 77300 69.8 7.21E+04 74.6 5.34E+04 66 34 2.51 3.48E+04 74.8 110000 68.5 1.05E+05 73.4 7.44E+04 65.3 34 3.98 5.09E+04 73.7 155000 67.3 1.52E+05 72.2 1.04E+05 64.6 34 6.31 7.39E+04 72.8 218000 66.1 2.20E+05 70.9 1.44E+05 64 34 10 1.07E+05 71.9 304000 64.8 3.14E+05 69.5 1.98E+05 63.5 34 15.8 1.53E+05 71 424000 63.6 4.47E+05 68.1 2.75E+05 63 34 25.1 2.20E+05 70.2 583000 62.5 6.29E+05 66.6 3.79E+05 62.5 34 39.8 3.14E+05 69.3 798000 61.3 8.75E+05 65.1 5.20E+05 62 34 63.1 4.45E+05 68.5 1080000 60.1 1.21E+06 63.6 7.13E+05 61.4 34 100 6.25E+05 68 1460000 59 1.65E+06 62.2 9.78E+05 60.6 46 0.1 213 88.2 510 86.9 352 87.3 638 82.4 46 0.158 336 87.5 799 86 558 86.7 970 80.9 46 0.251 526 86.8 1250 85.1 874 86.1 1460 79.5 46 0.398 818 85.9 1930 84.2 1360 85.5 2190 78.1 46 0.631 1270 84.9 2960 83 2100 84.9 3250 76.6 46 1 1960 83.9 4530 81.8 3250 84.2 4790 75.3 46 1.58 3000 82.8 6870 80.4 4990 83.4 7010 73.9 46 2.51 4570 81.7 10300 79.1 7630 82.6 10200 72.7 46 3.98 6920 80.5 15500 77.8 11600 81.8 14700 71.6 46 6.31 10400 79.4 22900 76.5 17700 80.9 21100 70.6 46 10 15600 78.4 33800 75.2 26800 80 30200 69.6 46 15.8 23200 77.3 49400 74 40100 79.1 42900 68.8 46 25.1 34100 76.3 71800 72.8 59600 78.1 60500 68.1 46 39.8 50500 75.4 104000 71.7 89400 77.1 85900 67.5 46 63.1 74100 74.5 149000 70.6 133000 76.1 121000 66.9 46 100 108000 73.6 213000 69.5 195000 75 170000 66.5

200 Table E-4. DSR Frequency Sweeps (continued). Binder: AAF-1 AAG-1 AAK-1 AAM-1 Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 10 0.1 3.34E+06 57.9 3.36E+06 70.6 1.28E+06 57.5 2.67E+06 45.8 10 0.158 4.62E+06 55.1 4.61E+06 68.1 1.73E+06 56.3 3.35E+06 44.3 10 0.251 6.17E+06 52.6 6.33E+06 65.5 2.32E+06 55 4.23E+06 42.7 10 0.398 8.09E+06 50.2 8.83E+06 62.5 3.06E+06 53.8 5.26E+06 41.3 10 0.631 1.04E+07 47.8 1.21E+07 59.4 4.07E+06 52.4 6.50E+06 40 10 1 1.34E+07 45.5 1.62E+07 56.2 5.34E+06 50.9 7.93E+06 38.7 10 1.58 1.67E+07 43.4 2.13E+07 53.1 6.98E+06 49.4 9.69E+06 37.6 10 2.51 2.09E+07 41.3 2.77E+07 50 8.99E+06 48 1.17E+07 36.5 10 3.98 2.58E+07 39.4 3.56E+07 46.9 1.14E+07 46.5 1.41E+07 35.6 10 6.31 3.12E+07 37.6 4.49E+07 43.9 1.44E+07 45 1.70E+07 34.6 10 10 3.77E+07 35.9 5.60E+07 41 1.80E+07 43.6 2.02E+07 33.7 10 15.8 4.51E+07 34.3 6.83E+07 38.3 2.24E+07 42.1 2.39E+07 32.9 10 25.1 5.37E+07 32.7 8.20E+07 35.8 2.76E+07 40.6 2.82E+07 32.1 10 39.8 6.31E+07 31.2 9.78E+07 33.3 3.39E+07 39.1 3.32E+07 31.2 10 63.1 7.34E+07 29.8 1.15E+08 31 4.13E+07 37.6 3.90E+07 30.4 10 100 8.51E+07 28.4 1.33E+08 28.8 4.98E+07 36.1 4.56E+07 29.5 22 0.1 2.89E+05 72.2 1.18E+05 83.7 1.38E+05 63.8 3.35E+05 57.1 22 0.158 4.19E+05 70.4 1.82E+05 82.6 1.92E+05 63 4.51E+05 55.4 22 0.251 6.00E+05 68.7 2.77E+05 81.6 2.64E+05 62.3 5.98E+05 53.9 22 0.398 8.49E+05 66.9 4.19E+05 80.4 3.63E+05 61.6 7.84E+05 52.5 22 0.631 1.19E+06 64.8 6.29E+05 79 4.96E+05 60.8 1.02E+06 51 22 1 1.65E+06 62.7 9.48E+05 77.4 6.76E+05 59.9 1.32E+06 49.6 22 1.58 2.27E+06 60.5 1.41E+06 75.6 9.17E+05 59 1.70E+06 48.3 22 2.51 3.07E+06 58.3 2.08E+06 73.5 1.24E+06 58.1 2.16E+06 47.1 22 3.98 4.12E+06 56.1 3.04E+06 71.3 1.67E+06 57.1 2.74E+06 46 22 6.31 5.45E+06 54 4.37E+06 68.8 2.23E+06 56.1 3.46E+06 44.8 22 10 7.12E+06 51.8 6.19E+06 66.1 2.96E+06 54.9 4.33E+06 43.8 22 15.8 9.20E+06 49.8 8.63E+06 63.2 3.91E+06 53.8 5.38E+06 42.8 22 25.1 1.18E+07 47.8 1.19E+07 60.3 5.13E+06 52.5 6.66E+06 41.8 22 39.8 1.50E+07 45.8 1.60E+07 57.2 6.72E+06 51.2 8.24E+06 40.9 22 63.1 1.88E+07 44 2.13E+07 54.2 8.69E+06 49.8 1.01E+07 39.9 22 100 2.33E+07 42.1 2.77E+07 51.1 1.12E+07 47.8 1.24E+07 38.7

201 Table E-4. DSR Frequency Sweeps (continued). Binder: AAF-1 AAG-1 AAK-1 AAM-1 Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 34 0.1 1.64E+04 80.7 5880 88.3 1.49E+04 71.3 2.16E+04 71.1 34 0.158 2.49E+04 80.2 9320 87.8 2.11E+04 70.1 3.05E+04 69.6 34 0.251 3.75E+04 79.5 14500 87.4 3.02E+04 69 4.32E+04 68.2 34 0.398 5.62E+04 78.5 22200 87 4.30E+04 68 6.09E+04 66.8 34 0.631 8.42E+04 77.3 34300 86.3 6.08E+04 67 8.53E+04 65.3 34 1 1.25E+05 76 53200 85.6 8.54E+04 66.1 1.19E+05 63.9 34 1.58 1.82E+05 74.6 82500 84.8 1.19E+05 65.3 1.64E+05 62.5 34 2.51 2.67E+05 73.1 127000 83.9 1.67E+05 64.6 2.25E+05 61.1 34 3.98 3.87E+05 71.5 195000 82.9 2.31E+05 63.9 3.06E+05 59.8 34 6.31 5.52E+05 69.9 297000 81.9 3.22E+05 63.2 4.13E+05 58.6 34 10 7.87E+05 68.1 451000 80.7 4.43E+05 62.5 5.55E+05 57.4 34 15.8 1.11E+06 66.3 682000 79.3 6.09E+05 61.8 7.39E+05 56.2 34 25.1 1.55E+06 64.3 1020000 77.8 8.34E+05 61 9.80E+05 55 34 39.8 2.13E+06 62.1 1520000 76 1.14E+06 60.2 1.29E+06 53.9 34 63.1 2.93E+06 60.5 2230000 74 1.55E+06 59.3 1.69E+06 52.9 34 100 3.97E+06 58.5 3220000 72 2.10E+06 58.4 2.21E+06 51.9 46 0.1 745 88.3 440 89.8 1460 80.4 968 84.3 46 0.158 1180 87.8 697 89.6 2210 79 1500 83.1 46 0.251 1850 87.3 1100 89.6 3310 77.7 2300 82 46 0.398 2900 86.7 1740 89.4 4910 76.4 3490 80.8 46 0.631 4510 86 2750 89.2 7210 75.1 5270 79.5 46 1 7010 85.2 4350 88.9 10600 73.8 7890 78.2 46 1.58 10900 84.3 6850 88.5 15300 72.6 11800 76.9 46 2.51 16700 83.4 10800 88.1 22200 71.5 17400 75.7 46 3.98 25600 82.4 16900 87.6 31800 70.5 25500 74.4 46 6.31 38900 81.3 26500 87.1 45500 69.6 37200 73.2 46 10 59000 80.2 41400 86.5 64700 68.8 53900 72 46 15.8 88700 79.1 64400 85.9 91700 68.1 77700 70.8 46 25.1 133000 77.9 99900 85.1 130000 67.5 111000 69.7 46 39.8 197000 76.6 154000 84.3 183000 66.9 158000 68.6 46 63.1 291000 75.3 238000 83.5 257000 66.3 224000 67.5 46 100 427000 73.9 364000 82.5 360000 65.8 316000 66.4

202 Table E-4. DSR Frequency Sweeps (continued). Binder: AC-5 AC-20 PG 70-22 Air Blown Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 10 0.1 3.01E+05 57.9 1.51E+06 54.1 3.11E+06 54 1.82E+06 54.1 10 0.158 4.09E+05 56.6 1.98E+06 53.2 4.15E+06 52.3 2.35E+06 53.2 10 0.251 5.49E+05 55.5 2.57E+06 52.2 5.43E+06 50.7 3.01E+06 52.2 10 0.398 7.29E+05 54.4 3.29E+06 51.3 7.03E+06 49.1 3.82E+06 51.3 10 0.631 9.61E+05 53.2 4.18E+06 50.2 9.01E+06 47.5 4.82E+06 50.2 10 1 1.26E+06 52.1 5.28E+06 49.1 1.15E+07 45.9 6.06E+06 49.1 10 1.58 1.64E+06 51 6.63E+06 47.9 1.45E+07 44.3 7.59E+06 47.9 10 2.51 2.13E+06 50 8.22E+06 46.8 1.81E+07 42.8 9.43E+06 46.8 10 3.98 2.74E+06 48.9 1.02E+07 45.7 2.25E+07 41.3 1.17E+07 45.7 10 6.31 3.52E+06 47.9 1.26E+07 44.5 2.76E+07 39.7 1.44E+07 44.5 10 10 4.48E+06 46.9 1.54E+07 43.4 3.38E+07 38.2 1.76E+07 43.4 10 15.8 5.67E+06 46 1.88E+07 42.3 4.09E+07 36.8 2.15E+07 42.3 10 25.1 7.14E+06 45 2.27E+07 41.2 4.92E+07 35.3 2.60E+07 41.2 10 39.8 9.00E+06 44 2.74E+07 40 5.88E+07 33.9 3.15E+07 40 10 63.1 1.12E+07 43.1 3.29E+07 38.9 6.96E+07 32.4 3.78E+07 38.9 10 100 1.39E+07 41.8 3.92E+07 37.8 8.18E+07 31 4.53E+07 37.8 22 0.1 3.25E+04 66.7 1.77E+05 56.4 3.01E+05 63.6 2.42E+05 56.4 22 0.158 4.56E+04 65.3 2.40E+05 56.5 4.15E+05 62.5 3.22E+05 56.5 22 0.251 6.34E+04 64.1 3.24E+05 56.6 5.70E+05 61.5 4.27E+05 56.6 22 0.398 8.75E+04 63 4.35E+05 56.6 7.79E+05 60.4 5.63E+05 56.6 22 0.631 1.20E+05 61.9 5.81E+05 56.4 1.06E+06 59.2 7.40E+05 56.4 22 1 1.64E+05 60.8 7.71E+05 56.1 1.43E+06 58 9.68E+05 56.1 22 1.58 2.24E+05 59.8 1.02E+06 55.7 1.92E+06 56.7 1.26E+06 55.7 22 2.51 3.03E+05 58.8 1.34E+06 55.2 2.56E+06 55.4 1.64E+06 55.2 22 3.98 4.09E+05 57.9 1.75E+06 54.6 3.39E+06 54.1 2.12E+06 54.6 22 6.31 5.48E+05 57 2.27E+06 53.9 4.45E+06 52.7 2.73E+06 53.9 22 10 7.31E+05 56.1 2.93E+06 53.2 5.81E+06 51.3 3.49E+06 53.2 22 15.8 9.70E+05 55.2 3.76E+06 52.4 7.51E+06 49.9 4.44E+06 52.4 22 25.1 1.28E+06 54.2 4.79E+06 51.5 9.67E+06 48.5 5.63E+06 51.5 22 39.8 1.69E+06 53.4 6.08E+06 50.4 1.23E+07 47 7.13E+06 50.4 22 63.1 2.21E+06 52.5 7.65E+06 49.6 1.56E+07 45.5 8.97E+06 49.6 22 100 2.88E+06 51.7 9.66E+06 48.7 1.96E+07 44 1.12E+07 48.7

203 Table E-4. DSR Frequency Sweeps (continued). Binder: AC-5 AC-20 PG 70-22 Air Blown Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 34 0.1 3030 77.1 1.71E+04 53.5 2.76E+04 71.9 3.10E+04 53.5 34 0.158 4480 75.5 2.45E+04 54.1 3.98E+04 70.6 4.30E+04 54.1 34 0.251 6560 74 3.47E+04 54.8 5.68E+04 69.5 5.93E+04 54.8 34 0.398 9520 72.5 4.87E+04 55.6 8.06E+04 68.4 8.13E+04 55.6 34 0.631 13700 71 6.80E+04 56.2 1.14E+05 67.4 1.10E+05 56.2 34 1 19600 69.6 9.46E+04 56.8 1.60E+05 66.4 1.49E+05 56.8 34 1.58 27800 68.3 1.31E+05 57.3 2.24E+05 65.4 2.01E+05 57.3 34 2.51 39100 67.1 1.80E+05 57.7 3.13E+05 64.5 2.70E+05 57.7 34 3.98 54700 66.1 2.46E+05 57.9 4.34E+05 63.6 3.61E+05 57.9 34 6.31 76200 65.2 3.34E+05 58.1 6.00E+05 62.6 4.81E+05 58.1 34 10 105000 64.3 4.52E+05 58.2 8.24E+05 61.6 6.39E+05 58.2 34 15.8 145000 63.6 6.09E+05 58.2 1.13E+06 60.6 8.44E+05 58.2 34 25.1 199000 62.9 8.18E+05 58 1.53E+06 59.4 1.11E+06 58 34 39.8 270000 62.4 1.09E+06 57.9 2.07E+06 58.3 1.47E+06 57.9 34 63.1 365000 62 1.45E+06 57.6 2.78E+06 57.2 1.92E+06 57.6 34 100 494000 61.8 1.92E+06 57.3 3.70E+06 56 2.50E+06 57.3 46 0.1 269 85.7 1710 61.8 2030 82.1 3660 61.8 46 0.158 419 84.6 2590 60.8 3100 80.7 5420 60.8 46 0.251 647 83.5 3900 59.6 4680 79.5 7910 59.6 46 0.398 991 82.3 5790 58.6 7010 78.3 11400 58.6 46 0.631 1500 81 8520 57.8 10400 76.9 16300 57.8 46 1 2270 79.6 12400 57.4 15400 75.7 23100 57.4 46 1.58 3410 78.1 18000 57.2 22600 74.4 32400 57.2 46 2.51 5060 76.7 25900 57.4 32900 73.3 45200 57.4 46 3.98 7470 75.3 37000 57.7 47700 72.3 62600 57.7 46 6.31 10900 74 52500 58.2 68800 71.3 86400 58.2 46 10 15900 72.8 74100 58.8 98700 70.4 118000 58.8 46 15.8 22900 71.7 104000 59.5 141000 69.6 162000 59.5 46 25.1 32800 70.6 145000 60.2 201000 68.8 221000 60.2 46 39.8 47100 69.8 202000 60.8 285000 68.1 300000 60.8 46 63.1 67000 68.9 281000 61.3 404000 67.3 406000 61.3 46 100 95000 68.2 388000 61.7 569000 66.6 549000 61.7

204 Table E-4. DSR Frequency Sweeps (continued). Binder: CRM Terpolymer SBS-LG Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 10 0.1 1.17E+06 54.1 3.60E+05 57.5 6.92E+05 54.1 10 0.158 1.50E+06 53.2 4.89E+05 57.2 9.24E+05 53.2 10 0.251 1.90E+06 52.2 6.58E+05 56.9 1.22E+06 52.2 10 0.398 2.39E+06 51.3 8.83E+05 56.6 1.59E+06 51.3 10 0.631 2.99E+06 50.2 1.18E+06 56 2.07E+06 50.2 10 1 3.73E+06 49.1 1.58E+06 55.4 2.67E+06 49.1 10 1.58 4.63E+06 47.9 2.10E+06 54.7 3.43E+06 47.9 10 2.51 5.71E+06 46.8 2.77E+06 53.9 4.38E+06 46.8 10 3.98 7.01E+06 45.7 3.66E+06 53.1 5.55E+06 45.7 10 6.31 8.57E+06 44.5 4.79E+06 52.1 6.99E+06 44.5 10 10 1.04E+07 43.4 6.25E+06 51.1 8.75E+06 43.4 10 15.8 1.26E+07 42.3 8.09E+06 50.1 1.09E+07 42.3 10 25.1 1.53E+07 41.2 1.05E+07 48.9 1.35E+07 41.2 10 39.8 1.84E+07 40 1.34E+07 47.7 1.66E+07 40 10 63.1 2.20E+07 38.9 1.71E+07 46.4 2.04E+07 38.9 10 100 2.63E+07 37.8 2.17E+07 45 2.48E+07 37.8 22 0.1 1.65E+05 56.4 4.71E+04 56.3 8.34E+04 56.4 22 0.158 2.16E+05 56.5 6.29E+04 56.8 1.12E+05 56.5 22 0.251 2.81E+05 56.6 8.42E+04 57.2 1.49E+05 56.6 22 0.398 3.65E+05 56.6 1.13E+05 57.7 1.99E+05 56.6 22 0.631 4.72E+05 56.4 1.52E+05 58 2.66E+05 56.4 22 1 6.10E+05 56.1 2.05E+05 58.2 3.56E+05 56.1 22 1.58 7.86E+05 55.7 2.77E+05 58.4 4.75E+05 55.7 22 2.51 1.01E+06 55.2 3.74E+05 58.4 6.31E+05 55.2 22 3.98 1.29E+06 54.6 5.06E+05 58.4 8.37E+05 54.6 22 6.31 1.64E+06 53.9 6.83E+05 58.3 1.11E+06 53.9 22 10 2.09E+06 53.2 9.21E+05 58 1.45E+06 53.2 22 15.8 2.64E+06 52.4 1.24E+06 57.6 1.90E+06 52.4 22 25.1 3.32E+06 51.5 1.66E+06 57 2.48E+06 51.5 22 39.8 4.16E+06 50.4 2.23E+06 56.4 3.21E+06 50.4 22 63.1 5.21E+06 49.6 2.98E+06 55.8 4.17E+06 49.6 22 100 6.51E+06 48.7 3.96E+06 55 5.36E+06 48.7

205 Table E-4. DSR Frequency Sweeps (continued). Binder: CRM Terpolymer SBS-LG Temp °C Freq, rad/s |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg |G*|, kPa Phase Angle, Deg 34 0.1 2.30E+04 53.5 8690 54.1 1.21E+04 53.5 34 0.158 3.05E+04 54.1 11500 54.3 1.59E+04 54.1 34 0.251 4.04E+04 54.8 15100 54.8 2.09E+04 54.8 34 0.398 5.34E+04 55.6 20000 55.3 2.77E+04 55.6 34 0.631 7.05E+04 56.2 26500 55.8 3.69E+04 56.2 34 1 9.33E+04 56.8 35300 56.5 4.93E+04 56.8 34 1.58 1.23E+05 57.3 47200 57.1 6.62E+04 57.3 34 2.51 1.62E+05 57.7 63300 57.8 8.90E+04 57.7 34 3.98 2.14E+05 57.9 85300 58.4 1.20E+05 57.9 34 6.31 2.81E+05 58.1 115000 59 1.62E+05 58.1 34 10 3.68E+05 58.2 156000 59.5 2.18E+05 58.2 34 15.8 4.82E+05 58.2 212000 59.9 2.94E+05 58.2 34 25.1 6.30E+05 58 289000 60.3 3.95E+05 58 34 39.8 8.21E+05 57.9 393000 60.5 5.32E+05 57.9 34 63.1 1.07E+06 57.6 535000 60.7 7.14E+05 57.6 34 100 1.38E+06 57.3 729000 61 9.59E+05 57.3 46 0.1 4570 61.8 2030 55.9 2010 61.8 46 0.158 6080 60.8 2700 55.3 2750 60.8 46 0.251 8060 59.6 3570 54.9 3730 59.6 46 0.398 10700 58.6 4700 54.7 5020 58.6 46 0.631 14200 57.8 6200 54.7 6710 57.8 46 1 18900 57.4 8180 54.9 8960 57.4 46 1.58 25300 57.2 10800 55.2 12000 57.2 46 2.51 33600 57.4 14300 55.8 16000 57.4 46 3.98 44800 57.7 19100 56.5 21400 57.7 46 6.31 59800 58.2 25500 57.3 28700 58.2 46 10 79600 58.8 34200 58.1 38600 58.8 46 15.8 106000 59.5 46200 58.9 52200 59.5 46 25.1 142000 60.2 62400 59.8 71000 60.2 46 39.8 189000 60.8 85300 60.6 96800 60.8 46 63.1 252000 61.3 117000 61.3 133000 61.3 46 100 335000 61.7 160000 61.9 182000 61.7

206 Table E-5. Results of SDENT Testing. Ext. to Total Ligament INIT Ext. to EMF 20 % Max. Load EXT20 Energy TEF Binder Temp. Width STIFF Max. Force FFPR Post Peak FFPR to Faiure FFPR C mm N/m mm mm N-m A 10 5 30.03 4.50 0.75 7.75 0.58 0.49 0.58 A 10 5 29.32 4.42 7.92 0.50 A 10 5 29.72 4.50 7.75 0.49 A 15 5 20.15 4.42 9.17 0.37 A 15 5 20.07 4.50 9.25 0.37 A 15 5 17.91 5.00 9.75 0.38 B 20 5 22.37 5.92 0.99 12.92 0.84 0.70 0.94 B 20 5 22.25 5.92 12.17 0.67 B 20 5 24.32 6.42 12.67 0.69 C 5 5 34.15 5.92 1.15 13.92 1.07 1.06 1.22 C 5 5 32.14 6.00 13.75 1.02 C 5 5 27.74 6.50 14.50 1.05 C 10 5 17.96 7.67 17.92 0.77 C 10 5 18.27 7.75 17.25 0.76 C 10 5 16.76 8.17 17.92 0.77 D 15 5 23.74 5.92 0.97 13.92 0.93 0.77 1.03 D 15 5 21.75 6.25 14.00 0.77 D 15 5 25.47 5.42 13.42 0.75 D 20 5 11.48 6.17 18.42 0.49 D 20 5 11.92 5.83 17.83 0.48 D 20 5 11.74 6.42 17.92 0.49 E 18 5 33.19 4.42 0.87 9.92 0.76 0.66 0.78 E 18 5 30.62 5.00 10.25 0.69 E 18 5 30.33 5.00 10.25 0.67 F 20 5 21.10 5.67 0.87 11.67 0.77 0.55 0.79 F 20 5 22.34 5.00 11.75 0.57 F 20 5 22.21 5.50 12.00 0.58 G 18 5 25.18 5.92 0.97 10.67 1.31 1.34 G 18 5 27.84 5.50 18.75 1.12 G 18 5 28.85 5.42 17.67 1.07 H 15 5 31.09 5.17 0.93 13.17 0.98 0.85 0.97 H 15 5 34.80 5.00 12.50 0.81 H 15 5 30.88 5.17 13.17 0.86 I 15 5 18.44 7.42 1.12 14.92 0.94 0.70 1.07 I 15 5 19.39 7.42 15.17 0.70 I 15 5 18.88 7.17 15.42 0.71 J 10 5 28.70 7.00 1.16 15.50 1.12 1.14 1.36 J 10 5 30.43 6.25 15.00 1.09 J 10 5 28.71 6.42 15.67 1.14 K 15 5 31.55 5.42 0.93 9.92 0.74 0.79 0.84 K 15 5 33.76 5.25 9.50 0.76 K 15 5 32.70 5.42 K 20 5 22.66 5.25 11.25 0.55 K 20 5 21.75 5.50 11.25 0.56 K 20 5

207 Table E-5. Results of SDENT Testing (continued). Ext. to Total Ligament INIT Ext. to EMF 20 % Max. Load EXT20 Energy TEF Binder Temp. Width STIFF Max. Force FFPR Post Peak FFPR to Faiure FFPR C mm N/m mm mm N-m L 25 5 20.31 6.17 1.02 8.67 0.58 0.44 0.72 L 25 5 17.42 6.83 10.33 0.51 L 25 5 18.01 7.08 9.33 0.45 M 10 5 23.32 8.25 1.28 15.00 1.02 0.99 1.35 M 10 5 25.65 7.67 15.67 1.05 M 10 5 22.33 7.42 14.92 0.98 N 5 5 27.47 5.50 0.89 9.25 0.63 0.59 0.70 N 5 5 29.13 4.75 8.50 0.54 N 5 5 27.12 5.08 8.58 0.56 O 15 5 32.35 6.25 1.17 14.50 1.11 1.19 1.36 O 15 5 33.56 6.50 14.50 1.21 O 15 5 P 25 5 17.10 6.00 0.92 13.25 0.81 0.55 0.92 P 25 5 16.79 6.50 13.50 0.56 P 25 5 15.79 14.50 0.58 K 15 15 53.89 8.50 0.92 31.25 0.73 4.83 0.80 15 15 48.30 9.33 31.50 4.77 15 15 46.23 9.25 30.50 4.48 20 15 27.70 11.00 38.42 3.15 20 15 30.12 10.50 39.25 3.33 20 15 30.42 10.50 39.25 3.26 O 10 15 46.22 12.75 1.23 33.58 0.90 7.84 1.42 10 15 52.10 12.17 39.25 7.42 10 15 42.69 13.17 39.75 7.51 15 15 27.46 13.17 50.92 5.87 15 15 27.13 15.25 51.00 6.06 15 15 27.32 13.75 49.25 6.12 A 10 15 40.40 8.92 0.84 26.83 0.58 3.31 0.60 10 15 43.82 8.50 27.50 3.23 10 15 39.49 8.75 27.75 3.16 15 15 24.64 9.50 31.00 2.22 15 15 28.44 9.83 30.08 2.15 15 15 26.62 9.50 31.00 2.20 AAA-1 5 15 24.53 12.67 1.02 70.92 1.25 3.85 1.08 5 15 21.38 12.00 70.50 3.93 5 15 24.12 10.50 71.00 3.94 AAB-1 10 15 26.78 9.58 0.81 51.33 0.96 3.56 0.88 10 15 28.56 9.00 50.75 3.59 10 15 28.85 8.67 50.67 3.55 AAC-1 10 15 41.57 7.17 0.69 49.42 1.05 4.43 0.84 10 15 43.34 7.50 47.00 4.30 10 15 41.99 7.08 47.58 4.44 AAD-1 5 15 32.43 14.67 1.34 52.67 1.06 5.58 1.19 5 15 34.64 13.75 52.00 5.50 5 15 36.03 15.25 51.75 5.43

208 Table E-5. Results of SDENT Testing (continued). Ext. to Total Ligament INIT Ext. to EMF 20 % Max. Load EXT20 Energy TEF Binder Temp. Width STIFF Max. Force FFPR Post Peak FFPR to Faiure FFPR C mm N/m mm mm N-m AAF-1 15 15 32.26 8.17 0.78 58.92 1.17 4.33 0.97 15 15 33.42 8.67 58.92 4.35 15 15 31.33 9.00 58.75 4.26 AAG-1 15 15 24.52 4.50 0.37 84.50 1.55 3.62 0.94 15 15 25.48 3.92 86.17 3.50 15 15 24.63 4.17 86.17 3.50 AAK-1 10 15 32.07 13.25 1.22 55.25 1.11 5.06 1.12 10 15 10 15 34.76 13.42 55.17 5.09 AAM-1 15 15 22.42 9.00 0.74 43.00 0.76 2.51 0.66 15 15 26.76 8.08 41.58 2.44 15 15 24.63 8.25 42.25 2.49 ALF AC-5 10 15 8.52 11.00 0.78 62.50 0.74 1.34 0.62 10 15 9.26 10.50 59.75 1.34 10 15 9.41 10.17 61.17 1.32 15 15 3.53 13.17 78.67 0.59 15 15 3.50 12.50 78.25 0.63 15 15 3.75 9.00 78.75 0.61 ALF AC-20 15 15 15.51 13.25 0.94 56.50 0.83 2.17 0.75 15 15 15.13 10.50 56.25 2.20 15 15 14.43 11.00 55.25 2.15 20 15 6.78 13.00 71.25 1.16 20 15 6.63 12.75 71.75 1.12 20 15 6.89 13.58 72.83 1.18 ALF PG 70-22 15 15 25.51 10.50 0.87 65.75 1.16 3.88 0.97 15 15 24.65 11.42 65.17 3.81 15 15 23.68 11.17 66.17 3.88 20 15 10.17 10.92 85.17 1.90 20 15 10.12 8.75 84.50 1.86 20 15 10.61 10.75 88.25 2.00 ALF Air Blown 15 15 16.82 13.00 1.09 54.75 0.83 2.48 0.82 15 15 17.34 14.00 55.00 2.60 15 15 17.38 13.42 51.42 2.57 20 15 8.30 15.25 65.50 1.42 20 15 8.50 13.25 64.25 1.44 20 15 ALF CR-TB 15 15 11.66 13.17 1.11 185.42 2.77 4.75 2.16 15 15 11.58 12.92 181.42 4.80 15 15 11.81 13.92 172.17 4.71 20 15 5.96 15.17 292.17 3.78 20 15 6.11 19.17 284.92 3.72 20 15 5.92 14.75 271.00 3.65

209 Table E-5. Results of SDENT Testing (continued). Ext. to Total Ligament INIT Ext. to EMF 20 % Max. Load EXT20 Energy TEF Binder Temp. Width STIFF Max. Force FFPR Post Peak FFPR to Faiure FFPR C mm N/m mm mm N-m ALF Terpolymer 15 15 4.13 318.42 21.95 340.92 3.24 6.05 5.34 15 15 3.96 313.25 341.00 6.39 15 15 4.22 272.58 307.83 5.76 20 15 1.89 370.67 447.92 4.48 20 15 1.96 432.25 467.25 4.59 20 15 1.97 370.42 482.42 4.92 ALF SBS-LG 15 15 7.45 13.25 17.25 304.02 3.10 14.19 8.56 15 15 6.67 13.33 303.65 12.65 15 15 7.93 13.17 303.77 13.56 20 15 3.24 477.67 303.91 10.00 20 15 3.17 492.08 304.04 10.77 20 15 3.48 494.83 303.80 11.87

210 Table E-6. Summary of LAS Test Data. Sweep Fatigue SVECD SVECD GFTAB Binder Temp. Time G* Exponent Strain FSC^ FSC FSC* C % Pa % % % %* A 15 300 1.71E+07 5.62 1.00 2.48 4.13 6.60 600 1.71E+07 5.62 2.50 4.12 4.37 6.60 900 1.71E+07 5.62 5.00 6.06 4.23 6.60 B 23 300 2.01E+07 5.14 1.00 7.79 4.62 5.79 600 2.01E+07 5.14 2.50 8.17 5.08 5.79 900 2.01E+07 5.14 5.00 8.46 5.19 5.79 C 11 300 1.95E+07 5.13 1.00 93.64 4.44 5.94 600 1.95E+07 5.13 2.50 41.31 5.10 5.94 900 1.95E+07 5.13 5.00 22.24 5.37 5.94 D 20 300 1.97E+07 5.05 1.00 3.70 4.19 5.89 600 1.97E+07 5.05 2.50 5.15 4.83 5.89 900 1.97E+07 5.05 5.00 6.61 4.92 5.89 E 22 300 2.07E+07 6.30 1.00 2.58 3.46 5.66 600 2.07E+07 6.30 2.50 4.11 3.50 5.66 900 2.07E+07 6.30 5.00 5.85 3.50 5.66 F 22 300 2.18E+07 5.61 1.00 3.15 3.64 5.42 600 2.18E+07 5.61 2.50 4.69 4.07 5.42 900 2.18E+07 5.61 5.00 6.34 3.98 5.42 G 22 300 2.08E+07 5.48 1.00 271.79 3.95 5.65 600 2.08E+07 5.48 2.50 84.61 4.05 5.65 900 2.08E+07 5.48 5.00 35.00 4.23 5.65 H 20 300 2.19E+07 5.91 1.00 17.69 3.41 5.41 600 2.19E+07 5.91 2.50 14.50 3.61 5.41 900 2.19E+07 5.91 5.00 12.48 3.87 5.41 I 17 300 2.22E+07 4.95 1.00 3.44 4.04 5.34 600 2.22E+07 4.95 2.50 5.10 4.66 5.34 900 2.22E+07 4.95 5.00 6.86 4.90 5.34 J 15 300 2.17E+07 5.31 1.00 10.82 3.97 5.44 600 2.17E+07 5.31 2.50 10.67 4.54 5.44 900 2.17E+07 5.31 5.00 10.55 4.69 5.44

211 Table E-6. Summary of LAS Test Data (Continued). Sweep Fatigue SVECD SVECD GFTAB Binder Temp. Time G* Exponent Strain FSC^ FSC FSC* C % Pa % % % %* K 23 300 1.71E+07 5.62 1.00 2.48 4.13 6.60 600 1.71E+07 5.62 2.50 4.12 4.37 6.60 900 1.71E+07 5.62 5.00 6.06 4.23 6.60 L 27 300 1.84E+07 6.38 1.00 0.97 3.66 6.22 600 1.84E+07 6.38 2.50 1.92 3.67 6.22 900 1.84E+07 6.38 5.00 3.21 3.85 6.22 M 11 300 1.86E+07 5.61 1.00 14.06 5.41 6.16 600 1.86E+07 5.61 2.50 14.00 5.68 6.16 900 1.86E+07 5.61 5.00 13.95 4.72 6.16 N 8 300 1.88E+07 6.68 1.00 7.37 3.43 6.11 600 1.88E+07 6.68 2.50 8.53 3.61 6.11 900 1.88E+07 6.68 5.00 9.53 3.68 6.11 O 22 300 2.30E+07 5.31 1.00 5.29 4.27 5.20 600 2.30E+07 5.31 2.50 6.73 4.48 5.20 900 2.30E+07 5.31 5.00 8.08 4.91 5.20 P 24 300 2.31E+07 5.85 1.00 1.71 3.34 5.17 600 2.31E+07 5.85 2.50 2.75 3.77 5.17 900 2.31E+07 5.85 5.00 3.94 3.79 5.17 AAA-1 7 300 2.83E+07 4.49 1.00 4.55 4.10 4.40 600 2.83E+07 4.49 2.50 5.81 4.72 4.40 900 2.83E+07 4.49 5.00 7.00 4.80 4.40 AAB-1 12 300 2.53E+07 5.05 1.00 2.77 3.76 4.81 600 2.53E+07 5.05 2.50 4.29 3.98 4.81 900 2.53E+07 5.05 5.00 5.97 4.23 4.81 AAC-1 14 300 2.63E+07 4.95 1.00 3.64 3.72 4.66 600 2.63E+07 4.95 2.50 4.85 4.00 4.66 900 2.63E+07 4.95 5.00 6.02 4.11 4.66 AAD-1 9 300 2.81E+07 4.56 1.00 4.06 3.88 4.43 600 2.81E+07 4.56 2.50 5.73 5.37 4.43 900 2.81E+07 4.56 5.00 7.44 5.14 4.43 AAF-1 19 300 2.79E+07 4.86 1.00 3.29 3.80 4.44 600 2.79E+07 4.86 2.50 4.54 4.10 4.44 900 2.79E+07 4.86 5.00 5.80 4.30 4.44

Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures Get This Book
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Traffic-associated fatigue damage is one of the major distresses in which flexible pavements fail. This type of distress is the result of many thousands—or even millions of wheel loads passing over a pavement.

The TRB National Cooperative Highway Research Program's pre-publication draft of NCHRP Research Report 982: Relationships Between the Fatigue Properties of Asphalt Binders and the Fatigue Performance of Asphalt Mixtures details these relationships and makes several conclusions and recommendations.

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