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Recent work by Gorsuch on oxidation of biological materials by combinations of nitric and perchloric acids; nitric, perchloric and sulfuric acids; and nitric and sulfuric acids all in the presence of sodium chloride has shown that chloride ion will not cause a loss of arsenic if sufficient nitric acid is initially present. All of the chloride is removed long before there is any chance of the arsenic being reduced to the trivalent form.
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