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Pages 56-59

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From page 56...
... 56 A p p e n d i x B This appendix presents generic procedures for the proposed spectroscopic methods. Those procedures were first implemented in the laboratory and then re-evaluated under field conditions.
From page 57...
... 57 entire ATR diamond surface and apply pressure to ensure full contact between the sample and the ATR diamond surface. For moldable materials, prepare self-supporting film before placing sample on the ATR diamond surface.
From page 58...
... 58 Control Sample Preparation The control sample is a sample of material with the designated chemical composition that is to serve as a reference for comparison to test samples. If the concentration of a chosen component in the designated mixture or solution is analyzed, several control samples should be prepared by mixing the component of interest with the neat (original)
From page 59...
... 59 XRD Testing Procedure The XRD testing procedure is as follows: • Prepare test sample as specified above. • Place sample into a sample holder.

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